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Superior ICP-OES optical design for unmatched speed and performance

Technical notes | 2016 | Agilent TechnologiesInstrumentation
ICP-OES
Industries
Manufacturer
Agilent Technologies

Summary

Significance of the topic


The rapid, simultaneous detection of multiple elements in complex matrices is a cornerstone of modern analytical chemistry. High-throughput methods that deliver accurate, precise, and reliable results are essential for environmental monitoring, quality control in manufacturing, clinical analysis, and research applications. The Agilent 5110 ICP-OES addresses these demands by combining advanced optical design with state-of-the-art detector technology to maximize performance and reduce operational costs.

Objectives and Overview


This technical overview describes the design and performance of the Agilent 5110 ICP-OES system. Key objectives include:
  • True simultaneous acquisition of the full 167–785 nm spectrum without sequential scanning
  • High resolution and low detection limits across all relevant emission lines
  • Automated optimization and background correction for simplified operation
  • Reduced warm-up time and gas consumption through hermetically sealed cooling

The article highlights how unique features such as Image Mapping (I-MAP) and Adaptive Integration Technology (AIT) deliver unmatched speed and data integrity.

Methodology and Instrumentation


Core components and technologies:
  • Vertical plasma torch with dual-view and synchronous dual-view pre-optics
  • Computer-optimized echelle polychromator with CaF2 cross-disperser
  • VistaChip II CCD detector featuring 70 diagonal linear arrays (DLAs) aligned to diffraction orders
  • Image Mapping Technology (I-MAP) to eliminate unused pixels and maximize throughput
  • Adaptive Integration Technology (AIT) for dynamic integration time adjustment per emission line
  • Hermetically sealed, −40 °C cooled detector requiring no argon purge

Main Results and Discussion


The 5110 ICP-OES achieves full-spectrum acquisition in under one second, with optical resolution better than 7 pm for wavelengths such as As 188.980 nm and Mo 202.032 nm. AIT automatically prevents signal saturation by adjusting read times, enabling simultaneous measurement of trace and major element concentrations in a single run. Anti-blooming drains on every pixel maintain accuracy in the presence of high-intensity signals. The hermetic cooling system reduces argon usage and startup delays.

Benefits and Practical Applications


Key advantages include:
  • Significantly increased sample throughput and reduced cost of ownership
  • Simultaneous internal standard and background correction for improved precision
  • Enhanced data integrity through multi-line confirmation without time penalty
  • Compatibility with hyphenated techniques such as chromatography and laser ablation

This makes the instrument ideal for environmental testing, pharmaceutical QA/QC, food safety, and materials research.

Future Trends and Opportunities


Advances in detector materials, machine-learning integration for real-time optimization, and miniaturized, portable ICP-OES systems are expected to expand on the 5110 platform’s capabilities. Integration with cloud-based data analysis and further improvements in spectral resolution will drive broader adoption across emerging fields such as metabolomics and nanomaterial characterization.

Conclusion


The Agilent 5110 ICP-OES with VistaChip II CCD detector represents a significant leap in simultaneous, full-spectrum elemental analysis. By combining innovative optical design, adaptive detection algorithms, and robust instrument engineering, it delivers unmatched speed, sensitivity, and reliability for a wide range of analytical challenges.

References


No additional literature references were provided in the source document.

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