<p><strong>Jiří Nováček, a researcher and the deputy director for research infrastructure at CEITEC Masaryk University, shares insights into his journey with Brnoregion Microscopy. Sparked by a conversation with Jan Neuman, Nováček saw the potential of integrating Atomic Force Microscopy (AFM) into life-science electron microscopy. Today, he plays an active role in the community, collaborating with colleagues to enhance educational initiatives.&nbsp;</strong></p><h4><strong>How did you become involved with Brnoregion Microscopy?</strong></h4><p>My involvement with Brnoregion Microscopy began through my interaction with <a target="_blank" rel="noopener noreferrer" href="https://brnoregion.com/en/news/people-of-brnoregion-microscopy-jan-neuman-nenovis">Jan Neuman</a>. We were discussing the potential applications of their integrated Atomic Force Microscopy (AFM) module in the field of life-science electron microscopy. I was immediately intrigued by the idea of forming a microscopy community and saw great potential in it. Jan's vision of fostering stronger local connections among colleagues with complementary expertise resonated with me. This alignment of interests and the shared goal of advancing our understanding and capabilities in microscopy made me eager to join and contribute to the community.&nbsp;</p><h4><strong>What role do you play in the community?</strong></h4><p>Currently, I am an active member of the Community working group within Brnoregion Microscopy. In this role, I collaborate closely with Tomáš Vystavěl from Thermo Fischer Scientific on various educational initiatives. Our focus is on enhancing the educational aspects of the Microscopy community, looking for opportunities for deepening the knowledge and skills in the area of microscopy in our region. It's a rewarding experience to be part of a team that is dedicated to fostering learning and innovation in this field.&nbsp;</p><h4><strong>What benefits does it bring to you?</strong></h4><p>Being part of the Microscopy community has been incredibly enriching for me. It provides a platform for continuous learning and exposure to the latest advancements in microscopy technology and techniques. Working together stimulates new ideas and approaches, which are key to our ongoing development. Additionally, it offers the opportunity to network with experts and peers, opening doors to potential collaborations and projects. That’s how it works in our local innovation ecosystem… &nbsp;</p><h4><strong>Do you have any message for the community?</strong></h4><p>Whether you're already involved or just curious, join the upcoming <a target="_blank" rel="noopener noreferrer" href="https://brnoregion.com/en/events/120-seconds-meet-brnoregion-microscopy-24-11">120 seconds: Meet Brnoregion Microscopy</a> event. It's a fantastic opportunity to see first-hand how the Microscopy community can benefit you. These events are designed to showcase the practical applications of microscopy and the innovative work being done by our members.&nbsp;</p>

People of Brnoregion Microscopy: Jiří Nováček (CEITEC MUNI)

<p><span style="color:#000000;"><strong>Brno, Czech Republic – Thursday, 17 October 2024 – Today, leading researchers from CEITEC Brno University of Technology unveiled a groundbreaking technological innovation: a state-of-the-art 329 GHz Electron Spin Resonance (ESR) spectrometer equipped with dynamic nuclear polarization (DNP) capabilities. This cutting-edge device, which has the&nbsp;potential to significantly advance materials science and molecular biology research, was presented during a grand unveiling ceremony attended by esteemed scientists and partners and held at CEITEC Masaryk University.</strong></span></p><p><span style="color:#000000;">The unveiling event featured opening remarks by <strong>Jiří Nantl</strong>, the Deputy Minister of Education, Youth and Sports of the Czech Republic and a former director of CEITEC Masaryk University (MU), <strong>Martin Weiter, </strong>the Vice-Rector for Research and Knowledge Transfer at Brno University of Technology (BUT), <strong>Radimír Vrba, </strong>the Director of CEITEC BUT, and <strong>Pavel Plevka</strong>, his counterpart at CEITEC MU. Following the opening words, <strong>Petr Neugebauer</strong>, the Principal Investigator from CEITEC BUT, solemnly unveiled the spectrometer and provided an in-depth explanation of its purpose and function.</span></p><h3><span style="color:#000000;"><strong>About the Spectrometer</strong></span></h3><p><span style="color:#000000;">The newly developed <strong>329 GHz Electron Spin Resonance Spectrometer</strong> is a significant leap forward in scientific instrumentation. This advanced tool is designed to measure electron spin resonance (ESR), a phenomenon that occurs when electrons absorb specific electromagnetic waves under the influence of a magnetic field. The spectrometer can offer researchers unprecedented insight into the structural and material properties of various substances, making it an essential tool in material science, chemistry, and biology.</span></p><p><span style="color:#000000;">What sets this spectrometer apart is its <strong>dual functionality</strong>: <strong>it can measure both ESR and liquid-state nuclear magnetic resonance (NMR) simultaneously</strong>. This dual capability is made possible by incorporating a magnet of an NMR spectrometer, streamlining the equipment and reducing costs by eliminating the need for a separate magnet in a new system. In addition, the spectrometer boasts <strong>fast frequency scanning</strong> of up to 10^16 Hz per second, offering unparalleled speed and precision in studying electron spin relaxation properties at microwave frequencies around 329 GHz.</span></p><figure class="image"><img style="aspect-ratio:1600/1068;" src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/CEITEC_Revolucni_spektrometr_pomuze_vedcum_porozumet_strukture_bilkovin_a_navrhnout_nove_leky_146bdac64f.jpeg" alt="CEITEC: Revoluční spektrometr pomůže vědcům porozumět struktuře bílkovin a navrhnout nové léky" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_CEITEC_Revolucni_spektrometr_pomuze_vedcum_porozumet_strukture_bilkovin_a_navrhnout_nove_leky_146bdac64f.jpeg 234w," sizes="100vw" width="1600" height="1068"></figure><h3><span style="color:#000000;"><strong>The team behind</strong></span></h3><p><span style="color:#000000;">This pioneering spectrometer is the result of a multi-disciplinary collaboration between scientists and international partners. The leader and principal investigator of the project is <strong>Petr Neugebauer</strong> (CEITEC BUT), with the critical NMR/EPR probe designed by <strong>Jan Dubský</strong> (CEITEC BUT), <strong>Petr Drexler</strong> and <strong>Martin Čáp</strong> (both FEEC BUT). The spectrometer’s quasi-optical bridge was supplied by <strong>Thomas Keating Ltd.</strong> (UK), while its 329 GHz components were sourced from <strong>Virginia Diodes Inc.</strong> (USA). The team, including <strong>Jan Dubský</strong> and <strong>Oleksii Laguta</strong> (CEITEC BUT), assembled and set up the device, with NMR tests conducted by <strong>Jan Dubský</strong> (CEITEC BUT) and <strong>Radovan Fiala</strong> (CEITEC MU).</span></p><p><span style="color:#000000;">The construction of the spectrometer was financed by the </span><a target="_blank" rel="noopener noreferrer" href="https://gacr.cz/en/"><span style="color:#000000;"><strong>Grant Agency of the Czech Republic (GAČR)</strong></span></a><span style="color:#000000;"><strong> EXPRO grant.</strong></span></p><h3><span style="color:#000000;"><strong>Impact and Practical Applications</strong></span></h3><p><span style="color:#000000;">The ultimate goal of the spectrometer is to enhance NMR experiments through dynamic nuclear polarization. This technique amplifies NMR signals by transferring polarization from electron spins to nuclei, allowing scientists to study biomolecules, such as proteins, with increased sensitivity. The device’s potential to advance molecular research holds promise for future applications in drug development, disease diagnosis, and other biomedical innovations.</span></p><figure class="image"><img style="aspect-ratio:1600/1068;" src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/CEITEC_Hedvika_Cimbalnikova_Revolucni_spektrometr_pomuze_vedcum_porozumet_strukture_bilkovin_a_navrhnout_nove_leky_Petr_Neugebauer_2062669b27.jpeg" alt="CEITEC/Hedvika Cimbálníková: Revoluční spektrometr pomůže vědcům porozumět struktuře bílkovin a navrhnout nové léky (Petr Neugebauer)" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_CEITEC_Hedvika_Cimbalnikova_Revolucni_spektrometr_pomuze_vedcum_porozumet_strukture_bilkovin_a_navrhnout_nove_leky_Petr_Neugebauer_2062669b27.jpeg 234w," sizes="100vw" width="1600" height="1068"></figure><h4><span style="color:#000000;"><strong>A Powerful Tool for Science</strong></span></h4><p><span style="color:#000000;">To put the spectrometer’s capabilities into perspective, it operates at frequencies 100 times higher than those used in mobile phones and generates a <strong>magnetic field 10 times stronger than those found in industrial scrap magnets</strong>. This immense power allows for the study of microscopic interactions that are essential to understanding complex biological and chemical processes.</span></p><p><span style="color:#000000;">For the general public, the unveiling of this spectrometer is an exciting step towards greater scientific discovery. Proteins, the building blocks of life, play a critical role in our body’s health and function. When proteins malfunction, diseases can arise. By using advanced magnetic resonance techniques, <strong>this spectrometer can help researchers better understand protein structures and design drugs</strong> that combat diseases at the molecular level.</span></p><p><span style="color:#000000;">Researchers involved in the project plan to publish their findings in leading scientific journals in the near future, showcasing the spectrometer’s far-reaching contributions to material sciences and molecular biology.</span></p><figure class="image"><img style="aspect-ratio:2900/647;" src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/CEITEC_Revolucni_spektrometr_pomuze_vedcum_porozumet_strukture_bilkovin_a_navrhnout_nove_leky_5_8e2ea29a10.jpg" alt="CEITEC: Revoluční spektrometr pomůže vědcům porozumět struktuře bílkovin a navrhnout nové léky" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_CEITEC_Revolucni_spektrometr_pomuze_vedcum_porozumet_strukture_bilkovin_a_navrhnout_nove_leky_5_8e2ea29a10.jpg 245w," sizes="100vw" width="2900" height="647"></figure>

Revolutionary spectrometer will help scientists understand protein structure and design new drugs

<p><strong>In the week of January 6, the following webinars await you in the field of atomic and molecular spectroscopy and spectrometry.</strong></p><p><strong>We bring you also a selection of the TOP 10 most requested webinars in the field of atomic and molecular spectroscopy and spectrometry on LabRuleICPMS portals in 2024.</strong></p><blockquote><p><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinars"><strong>👉 DETAILS AND REGISTRATION IN THE WEBINARS SECTION</strong></a></p><p><strong>👉 Search and filter in the largest global database</strong> with over <strong>3 500 GC, LC, MS and spectroscopy webinars</strong>.</p></blockquote><h4><strong>Week 2/2025</strong></h4><h5><strong>1. Agilent Technologies: Intelligent Analysis of Wastewaters using an Agilent ICP-MS with Integrated Autodilutor</strong></h5><div><div><ul><li><div>Tu, 7.1.2025 09:30 CET</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/4542">Registration</a></div></li></ul></div><p>Come to learn about how the analysis of wastewater made easy with the new Agilent ICPMS integrated autodilutor.</p></div><h5><strong>2.&nbsp;Anton Paar: Indentation Optimization - Soft Materials</strong></h5><div><div><ul><li><div>Tu, 7.1.2025 18:00</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/4375">Registration</a></div></li></ul></div><p>This webinar focuses on the mechanical behavior of soft materials such as tissues, gels, and polymers, and provides practical strategies for obtaining high-quality indentation data from these materials.</p></div><h5><strong>3.&nbsp;Anton Paar: Discover Quality Control with a Refractometer in the Chemical Industry</strong></h5><div><div><ul><li><div>Fr, 10.1.2025 09:00 CET</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/4577">Registration</a></div></li></ul></div><p>In this webinar, Anton Paar will showcase the significant benefits of using a refractometer for quality control in chemical industry laboratories.</p></div><h4><strong>TOP 10 in 2024</strong></h4><h5><strong>1. Agilent Technologies: Ready to replace your 7700? The latest 7850 or 7900 will exceed your expectations! Part 1</strong></h5><div><div><ul><li><div><span style="color:#D92B04;">RECORD</span> | Already taken place Tu, 28.3.2023</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/2481">Registration</a></div></li></ul></div><p>Join us in this two-part webinar series to find out what the new generations of Agilent single quadrupole systems: 7850 ICPMS, and 7900 ICPMS have to offer.</p></div><h5><strong>2.&nbsp;Agilent Technologies: Winter Plasma Conference 2024 Highlights on Agilent ICP-OES and ICP-MS Applications: Part 2</strong></h5><div><div><ul><li><div><span style="color:#D92B04;">RECORD</span> | Already taken place Fr, 2.2.2024</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/3142">Registration</a></div></li></ul></div><p>New and exciting instrumentations and applications in the atomic spectroscopy area.</p></div><h5><strong>3.&nbsp;Agilent Technologies: Minimize Carry Over and Contamination on Your Agilent ICP-MS</strong></h5><div><div><ul><li><div><span style="color:#D92B04;">RECORD</span> | Already taken place Tu, 22.8.2023</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/2788">Registration</a></div></li></ul></div><p>Techniques and tools for improve wash out of “sticky” elements, such as B, Tl, and Hg, on an Agilent ICP-MS will be discussed.</p></div><h5><strong>4.&nbsp;Agilent Technologies: ICP Expert How To: What is it and How to set up an Advanced Valve System (AVS) for ICP-OES</strong></h5><div><div><ul><li><div><span style="color:#D92B04;">RECORD</span> | Already taken place Fr, 12.5.2023</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/2567">Registration</a></div></li></ul></div><p>This presentation will discuss the different types of interferences present in ICP and how to correct for them.</p></div><h5><strong>5.&nbsp;Thermo Fisher Scientific: How to use Inter Element Correction (IEC) to Overcome Interferences in ICP-OES</strong></h5><div><div><ul><li><div><span style="color:#D92B04;">RECORD</span> | Already taken place We, 4.12.2024</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/4197">Registration</a></div></li></ul></div><p>How you can deal with complex spectral interferences on ICP-OES by using Inter Element Correction (IEC) in an easy and simple way.</p></div><h5><strong>6.&nbsp;PerkinElmer: Semiconductor Specialty Gas Analysis Using GDI-ICP-MS</strong></h5><div><div><ul><li><div><span style="color:#D92B04;">RECORD</span> | Already taken place Th, 27.6.2024</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/4046">Registration</a></div></li></ul></div><p>You will learn about an alternative sample prep method using a gas exchange device.</p></div><h5><strong>7.&nbsp;Agilent Technologies: How to Minimize Contamination and Carry Over Issues on ICP-MS</strong></h5><div><div><ul><li><div><span style="color:#D92B04;">RECORD</span> | Already taken place Su, 1.1.2023</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/3832">Registration</a></div></li></ul></div><p>Sources of common lab contaminants in ICP-MS and methods used for their elimination.</p></div><h5><strong>8.&nbsp;Agilent Technologies: Agilent M Lens for ICP-MS and the Semiconductor Industry</strong></h5><div><div><ul><li><div><span style="color:#D92B04;">RECORD</span> | Already taken place Th, 8.8.2024</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/3907">Registration</a></div></li></ul></div><p>Agilent M Lens for ICP-MS and the Semiconductor Industry</p></div><h5><strong>9.&nbsp;Agilent Technologies: Direct Elemental Analysis of Edible Oils Using an Agilent 5800 ICP-OES</strong></h5><div><div><ul><li><div><span style="color:#D92B04;">RECORD</span> | Already taken place Th, 11.7.2024</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/3898">Registration</a></div></li></ul></div><p>Direct Elemental Analysis of Edible Oils Using an Agilent 5800 ICP-OES</p></div><h5><strong>10.&nbsp;Agilent Technologies: Troubleshooting Tips and Tricks in Single Quad and Triple Quad ICP-MS</strong></h5><div><div><ul><li><div><span style="color:#D92B04;">RECORD</span> | Already taken place Fr, 1.3.2024</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/3143">Registration</a></div></li></ul></div><p>Most common tips and tricks on troubleshooting Agilent ICPMS, both single quad and triple quad.</p></div>

Webinars LabRulezICPMS Week 2/2025 + TOP 10 in 2024

<p><strong>On October 4, 2024, Professor Josef Dadok, the founder of nuclear magnetic resonance (NMR) in Czechoslovakia and a prominent figure in the field internationally, died in the United States at the age of 98. Professor Dadok worked in Brno in the 1950s and 1960s, where he led the development of the first NMR spectrometers at the Institute of Instrumentation of the Czechoslovak Academy of Sciences, later mass-produced by the national company Tesla Brno, making Czechoslovakia one of the world leaders in this field.</strong></p><p>In 1967 Josef Dadok went to the USA for a work placement, from where he did not return due to political developments in Czechoslovakia after 1968, but where he continued to develop NMR technologies at Carnegie Mellon University in Pittsburgh. Here he developed the first superconducting spectrometer with a magnetic field of 14.1 T and an operating frequency of 600 MHz, which was for many years the most powerful device of its kind.</p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/CEITEC_Pamatka_Josefa_Dadoka_zije_na_CEITEC_dal_prostrednictvim_spickoveho_vyzkumu_v_oblasti_spektroskopie_3_bf932352cd.jpg" alt="CEITEC: The memory of Josef Dadok lives on at CEITEC through cutting-edge research in spectroscopy" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_CEITEC_Pamatka_Josefa_Dadoka_zije_na_CEITEC_dal_prostrednictvim_spickoveho_vyzkumu_v_oblasti_spektroskopie_3_bf932352cd.jpg 125w," sizes="100vw" width="961" height="1201"></p><p>In 2013, Professor Dadok was awarded an honorary doctorate from Masaryk University and Brno University of Technology for his outstanding contribution to Czechoslovak science and technology. The National Centre for Nuclear Magnetic Resonance CEITEC MUNI bears his name in his honour. <a target="_blank" rel="noopener noreferrer" href="https://nmr.ceitec.cz/?_gl=1*pzdx3f*_ga*ODg2MDE3MjgzLjE3MzU4MzczMjI.*_ga_L74QG6CYBE*MTczNjE4ODMyMS4yLjAuMTczNjE4ODMyMS4wLjAuMA.."><i>"The Josef Dadok National NMR Centre</i></a><i> was inaugurated in 2013 with the personal participation of Prof. Dadok and still serves users from all over the world. Its name commemorates Josef Dadok's fundamental contribution to the development of this technology not only in Czechoslovakia but also on the international scene,"</i> says <a target="_blank" rel="noopener noreferrer" href="https://www.ceitec.eu/radovan-fiala/u17058?page=publication">Radovan Fiala</a>, who started his professional career at the Institute of Instrumentation of the CAS in Brno, in the department founded by Josef Dadok.</p><p><i>"The pioneering work of Josef Dadok has been followed up by the development of a spectrometer that can simultaneously measure electron spin resonance and nuclear magnetic resonance by revolutionary fast scanning. Our instrument will serve interdisciplinary research at the Josef Dadok National NMR Centre at CEITEC MUNI,"</i> adds <a target="_blank" rel="noopener noreferrer" href="https://www.ceitec.eu/petr-neugebauer/u91434?page=publication">Petr Neugebauer</a>, head of the magneto-optical and THz spectroscopy research group at CEITEC BUT.</p><p>Many other scientists also keep Josef Dadok's legacy in spectroscopy alive and continue to build on this legacy, as Professor Josef Dadok was not only an outstanding scientist and engineer, but also an inspiring mentor and colleague who influenced many generations of researchers.</p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/CEITEC_Pamatka_Josefa_Dadoka_zije_na_CEITEC_dal_prostrednictvim_spickoveho_vyzkumu_v_oblasti_spektroskopie_2_5bfe3171b6.jpeg" alt="CEITEC - The memory of Josef Dadok lives on at CEITEC through cutting-edge research in spectroscopy" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_CEITEC_Pamatka_Josefa_Dadoka_zije_na_CEITEC_dal_prostrednictvim_spickoveho_vyzkumu_v_oblasti_spektroskopie_2_5bfe3171b6.jpeg 235w," sizes="100vw" width="1600" height="1067"></p>

The memory of Josef Dadok lives on at CEITEC through cutting-edge research in spectroscopy

<p><strong>Our Library never stops expanding. What are the most recent contributions to LabRulezICPMS Library in the week of 6th January 2025? Check out new documents from the field of spectroscopy/spectrometry and related techniques!</strong></p><blockquote><p><span style="font-size:20px;">👉 </span><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/library"><span style="font-size:20px;"><strong>SEARCH THE LARGEST REPOSITORY OF DOCUMENTS ABOUT SPECTROSCOPY/SPECTROMETRY RELATED TECHNIQUES</strong></span></a></p></blockquote><blockquote><p><strong>👉 Need info about different analytical techniques?</strong> Peek into <a target="_blank" rel="noopener noreferrer" href="https://lcms.labrulez.com/library"><strong>LabRulezLCMS</strong></a> or <a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/library"><strong>LabRulezGCMS</strong></a> libraries.</p></blockquote><p>This week we bring you applications by <strong>ALS Europe</strong>, <strong>Thermo Fisher Scientific,</strong> <strong>Agilent Technologies and</strong> <strong>Shimadzu</strong>!</p><h4><strong>1. ALS Europe: Precision and Detail Ensured by Scanning Electron Microscopy</strong></h4><ul><li>Technical note</li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/labrulez-bucket-strapi-h3hsga3/enviromail_19_europe_precision_and_detail_ensured_by_scanning_electron_microscopy_july2024_f03db63b86.pdf"><strong>Full PDF for download</strong></a></li></ul><p>A Scanning Electron Microscope equipped with Energy-Dispersive X-ray Spectroscopy (SEM-EDS) represents a powerful tool and robust analytical technique that offers an extensive array of data regarding the microstructural and compositional attributes of a diverse spectrum of materials. ALS Laboratories are equipped with a modern scanning electron microscope Tescan VEGA 3 LMU with an energy-dispersive detector (EDS) Oxford X-Max 20. It is an ideal technique for surface inspection, identification of the elemental composition of unknown particles in a sample, or advanced determination of particle size or type distribution.</p><h5><strong>Elemental Analysis</strong></h5><p>An effective complement to the microscope itself is the aforementioned EDS detector, which can detect characteristic X-rays and assign them to specific elements. The latest systems are capable of detecting elements heavier than boron, i.e., elements with an atomic number &gt;5. The Oxford AZtec X-Max 20 EDS detector in our laboratories can very quickly confirm or exclude the presence of elements heavier than beryllium (excluding hydrogen, helium, and lithium). The result is a spectrum from which the composition of the examined particle can be determined. This capability can be utilised, for example, to compare the sample material with a supplied standard or to observe changes occurring in the sample when exposed to various processes and conditions.</p><h5><strong>Feature Analysis</strong></h5><p>Using the software module "Feature Analysis," it is possible to automatically analyse a large number of particles in terms of morphology, chemical composition, or a combination of both. A significant advantage over common techniques such as laser diffraction is the ability to directly image the analysed particles. The particles can be sorted entirely automatically, either by morphology, by defining parameters such as length, area, shape, etc., or by chemical composition, for example, whether they contain a specific element or not. The outputs can include various graphs and tables (see Figures 4 (A/B).</p><p><strong>The most common analyses in ALS Laboratories include: the anti-corrosion coating of car parts, the specification of foreign particles, a very frequent analysis is an identification of deposits on filters, identification of sediments, or stains, and defects on the surface of various materials and products. SEM-EDS analysis is also often an integral part of production processes, where quality control of intermediate and final products is crucial.</strong></p><h4><strong>2. Thermo Fisher Scientific: Analysis of photovoltaic grade silicon using triple quadrupole inductively coupled plasma mass spectrometry (ICP-MS)</strong></h4><ul><li>Application</li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/labrulez-bucket-strapi-h3hsga3/an_003016_tea_icp_ms_icap_mtx_photovoltaics_an003016_em_en_27bac73d30.pdf"><strong>Full PDF for download</strong></a></li></ul><p><strong>To demonstrate a robust and accurate analytical method for the determination of bulk and trace elements in photovoltaic samples using triple quadrupole ICP-MS</strong></p><h5><strong>Introduction</strong></h5><p>Development of renewable and low-carbon energy sources has become critical in addressing global concerns related to carbon emissions and climate change. One key technology in achieving the reduction of CO<sub>2</sub> emissions while ensuring a stable and reliable energy supply is the use of photovoltaic (PV) technology. PV technology harnesses the natural energy from the sun and converts it into electrical power, emits zero CO<sub>2</sub>, and enhances energy security. Additionally, PV solar cells are predominantly composed of silicon, an abundant resource on Earth, making the transition to PV energy a viable option as a primary source of electricity, aligning with the move towards climate-friendly energy resources.</p><p>However, it is important to acknowledge that PV also has certain drawbacks, including susceptibility to damage, dependence on sunlight, and associated costs. To address these concerns, it is crucial to focus on developing innovative solutions that result in durable products, increased energy efficiency, and degradation prevention.</p><h5><strong>Experimental optimization of the instrument parameters</strong></h5><p>An <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/products/1488"><strong>iCAP MTX ICP-MS</strong></a>, operated together with a Thermo Scientific™ iSC-65 Autosampler, was used for all analyses. The sample introduction system consisted of a Peltier-cooled (at 2.7 °C) and dedicated HF sample introduction kit consisting of a baffled PFA cyclonic spray chamber (Savillex, Eden Prairie, MN, USA), PFA concentric nebulizer (Savillex), and PLUS torch1 with a 2.0 mm i.d. removable sapphire injector. The built-in argon humidifier was used for moisturizing the nebulizer gas to prevent salt deposit on the<br>nebulizer tip, along with integrated argon gas dilution.&nbsp;</p><p>To further increase uptime of the instrument, intelligent matrix handling was used, a unique feature of the <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/products?instrumentationItems=83&amp;search=MSX+MTX"><strong>Thermo Scientific™ iCAP™ MX Series ICP-MS instruments</strong></a> to reduce exposure to sample matrix during sample uptake and wash. Interferences on all analytes were effectively controlled using the QCell collision/reaction cell (CRC) and leveraging the superior interference removal capabilities of a triple quadrupole ICP-MS instrument. In addition to the use of O<sub>2</sub> as a reactive gas in triple quadrupole mode for highly interfered analytes such as phosphorus, sulfur, arsenic and selenium, the instrument was also operated in single quadrupole mode using helium and kinetic energy discrimination (KED) for interference free analysis of other analytes over the full mass range. Table 1 summarizes the instrument configuration and analytical parameters.</p><p>The selection of the most appropriate isotopes per analyte, as well as the optimum analysis conditions (i.e., KED mode versus reactive gas, on mass mode versus mass shift mode) was automatically accomplished using the Reaction Finder Method Development Assistant available in the <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/products/1489"><strong>Thermo Scientific™ Qtegra™ Intelligent Scientific Data Solution™ (ISDS) Software</strong></a>. Measurement modes were optimized using the provided autotune procedures.</p><p>The iSC-65 Autosampler allowed for the use of Step Ahead functionality to shorten the overall measurement time per sample and increase the number of samples that can be analyzed per unit time.</p><h4><strong>3. Agilent Technologies: ICP-OES Analysis of Electrolytes for All-Vanadium Redox Flow Batteries</strong></h4><ul><li>Application</li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/labrulez-bucket-strapi-h3hsga3/application_v_flow_battery_icp_oes_5800_5994_7968en_agilent_1_563bab0388.pdf"><strong>Full PDF for download</strong></a></li></ul><p><strong>Quantification of impurity elements in vanadium sulfate electrolytes using an Agilent 5800 VDV ICP-OES.</strong></p><p>The detrimental effects of burning fossil fuels on the climate, environment, and air quality are driving the shift towards cleaner and more sustainable sources of energy. However, challenges remain for the renewable energy sector, as both wind and solar power can be intermittent, leading to fluctuations in energy generation. To offset the uncontrollable nature of these weather-based technologies, there is increasing demand for large-scale energy storage solutions to balance the requirements of energy grids. Addressing these challenges is crucial for achieving sustainable, reliable, and secure systems that can meet both current and future energy needs.</p><p>Compared to traditional batteries, which store energy in the electrodes, flow batteries are electrochemical (redox) systems that store and release energy through chemical reactions within the electrolyte. This mechanism means that the capacity and power of flow batteries can be tailored separately, providing scalability and long lifespans. This flexibility makes them suitable for grid-scale energy storage and backup power systems.</p><h5><strong>Instrumentation</strong></h5><p>Elemental analysis of the samples was carried out using the Agilent 5800 VDV ICP-OES. The instrument was fitted with a SeaSpray glass concentric nebulizer, double-pass cyclonic spray chamber, and an Easy-fit fully demountable torch with 1.8 mm quartz injector.</p><p>Agilent ICP Expert software was used to control the 5800 ICP-OES, optimize and run the method, and to process the data.</p><h5><strong>Automatic background correction</strong></h5><p>The Fitted Background Correction (FBC) routine within the ICP Expert software was used for all elements in this study. FBC uses a sophisticated mathematical algorithm to automatically model and subtract simple and complex background structures produced by non-analyte signals.</p><h5><strong>Conclusion</strong></h5><p>The Agilent 5800 VDV ICP-OES successfully determined 11 impurity elements in four all-vanadium flow battery electrolytes—an important quality control application within the battery production process. The main advantages of the analytical method include:</p><ul><li>Good calibration linearity (R&gt;0.9999) and low method detection limits (&lt;0.09 mg/L) for all target analytes.</li><li>Confirmation of the method’s accuracy demonstrated by 94 to 103% recoveries of 0.5 mg/L spikes added to one of the commercial vanadium sulfate electrolyte samples.</li><li>Recovery of all elements within 100 ±10% indicating that the 5800 can tolerate the high concentration of vanadium in the electrolyte samples, due to its robust vertical plasma and SSRF generator.</li><li>Excellent instrument stability, as shown by the precision of repeated measurements of a commercial electrolyte sample over four hours (RSDs &lt; 2.3%).</li></ul><p><strong>The 5800 VDV ICP-OES method is suitable for the accurate quantification of some key impurity elements in electrolytes used in all-vanadium flow batteries, in accordance with China standard method GB/T 37204-2018.</strong></p><h4><strong>4. Shimadzu: Observation of Rubber Fatigue Testing Specimens Using Two Types of X-Ray CT Systems</strong></h4><ul><li>Application</li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/labrulez-bucket-strapi-h3hsga3/an_01_00740_en_9631abda15.pdf"><strong>Full PDF for download</strong></a></li></ul><h5><strong>User Benefits</strong></h5><ul><li>The volume and shape of individual micro-defects in rubber can be observed in detail using a microfocus X-ray CT system.</li><li>The approximate position and size of microcracks can be determined efficiently using a phase-contrast X-ray CT system.</li><li>The progression status of defects and cracks in rubber can be compared at respective cycle counts of fatigue testing.</li></ul><p>Rubber products serve an important role in a wide range of fields, such as automotive tires, industrial products, and medical devices. However, functional losses can occur due to fatigue and aging after long periods of use. Therefore, evaluating the durability of rubber is an important issue.</p><p>In order to evaluate the progression of defects during usage, rubber must be inspected before it fails. It can be inspected by cutting it apart, but non-destructive inspections are preferable due to the disadvantages of destructive inspections, such as the inability to restore specimens after inspections and the limitation of only being able to evaluate cut surfaces.</p><p>Internal defects can be detected and three-dimensionally observed using an X-ray CT system. One X-ray imaging method typically used is absorption imaging, which generates images based on the quantity of X-rays absorbed. Another method is phase imaging, which is a new unconventional method that generates images based on variations in the phase of X-rays. This article describes using two types of instruments based on those different imaging methods to observe rubber during fatigue testing (Table 1).</p><h5><strong>Conclusion</strong></h5><p>Specimens for testing rubber fatigue were scanned using two types of X-ray imaging systems, a microfocus X-ray CT system and a phase-contrast X-ray CT system. By stretching samples, magnified images were acquired by the inspeXio SMX-225CT FPD HR Plus X-ray CT inspection system, and even small defects could be observed in detail and defect volume and count values compared at respective cycle count levels. The Xctal 5000 can determine the approximate orientation, size, and depth of microcracks without stretching samples or using magnified imaging. Both instruments can inspect items non-destructively, and the same specimen can be used to understand the progression of defects and cracks at any number of cycles. The characteristics of these instruments for scanning and analyzing data from specimens tested for rubber fatigue are indicated in Table 7.</p>

News from LabRulezICPMS Library - Week 2, 2025

<p><strong>In the week from January 13, the following webinars await you in the field of atomic and molecular spectroscopy and spectrometry</strong></p><blockquote><p><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinars"><strong>👉 DETAILS AND REGISTRATION IN THE WEBINARS SECTION</strong></a></p><p><strong>👉 Search and filter in the largest global database</strong> with over <strong>3 500 GC, LC, MS and spectroscopy webinars</strong>.</p></blockquote><h5><strong>1. Anton Paar: How Sweet It Is: Innovations and Automation in Sugar and Chocolate Analysis</strong></h5><div><div><ul><li><div>Tu, 14.1.2025 18:00 CET</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/4448">Registration</a></div></li></ul></div><p>This webinar describes a comprehensive approach to analyzing sugar, confectionary products, and chocolate.</p></div><h5><strong>2.&nbsp;Shimadzu Corporation: Elemental Analysis: Energize the Future with Advanced Battery Testing Solutions</strong></h5><div><div><ul><li><div>Tu, 14.1.2025 19:00 CET</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/4668">Registration</a></div></li></ul></div><p>Innovative techniques for overcoming unique matric-specific challenges for analyzing black mass, electrolyte solutions, anode materials, and cathode materials by ICP-AES, TOC, and X-ray fluorescence.</p></div><h5><strong>3.&nbsp;Agilent Technologies: Automating the Workflow for the Analysis of Soils by ICP-OES. Less Work, More Flow</strong></h5><div><div><ul><li><div>Tu, 14.1.2025 21:30 CEST</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/3770">Registration</a></div></li></ul></div><p>ADS2 automates lab workflows, from calibrators to smart dilutions. Faster, smarter, and more accurate.</p></div><h5><strong>4.&nbsp;Agilent Technologies: Agilent 8700 LDIR Workflows</strong></h5><div><div><ul><li><div>Th, 16.1.2025 20:00 CET</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/4637">Registration</a></div></li></ul></div><p>The two main worklflows of the LDIR will be discussed and demonstrated.</p></div>

Webinars LabRulezICPMS Week 3/2025

<p><strong>Our Library never stops expanding. What are the most recent contributions to LabRulezICPMS Library in the week of 13th January 2025? Check out new documents from the field of spectroscopy/spectrometry and related techniques!</strong></p><blockquote><p><span style="font-size:20px;">👉 </span><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/library"><span style="font-size:20px;"><strong>SEARCH THE LARGEST REPOSITORY OF DOCUMENTS ABOUT SPECTROSCOPY/SPECTROMETRY RELATED TECHNIQUES</strong></span></a></p></blockquote><blockquote><p><strong>👉 Need info about different analytical techniques?</strong> Peek into <a target="_blank" rel="noopener noreferrer" href="https://lcms.labrulez.com/library"><strong>LabRulezLCMS</strong></a> or <a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/library"><strong>LabRulezGCMS</strong></a> libraries.</p></blockquote><p>This week we bring you applications by <strong>ALS Europe</strong>, <strong>Thermo Fisher Scientific,</strong> <strong>Agilent Technologies and</strong> <strong>Shimadzu</strong>!</p><h4><strong>1. ALS Europe:&nbsp;Isotope Ratio Analysis Solves Complex Problems</strong></h4><ul><li>Technical note</li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/paper/28592"><strong>Full PDF for download</strong></a></li></ul><p>ALS Laboratories are one of the few in the world to offer commercial isotope ratio testing services not only for radiogenic systems (Sr, Nd, Pu, U) and light stable isotopes (Li, B, Si), but also for heavy stable elements such as Ag, Ca, Cd, Cu, Fe, Mg, Mo, Si, and Zn.</p><p>All of these isotope ratio tests can be used as a fingerprint to provide information about origin or geologica<strong>l age, and have potential to be used for tracing pollution and exposure sources.</strong></p><h5><strong>ALS Capabilities for Isotope Ratio Analysis</strong></h5><p>ALS experts have more than 30 years of research and commercial testing experience for stable isotope ratio analysis using both High Resolution Sector Field ICP-MS (ICP-SFMS) and Multi-Collector ICP-MS (MC-ICP-MS) instrumentation. Our expert team has made substantial contributions to the field of isotope ratio analysis with 170 peer-reviewed publications. ALS laboratories offer isotope ratio analyses for more than 20 stable and radiogenic isotopic systems in a variety of sample matrices with high precision, even where sample concentrations are very low.</p><h4><strong>2. Thermo Fisher Scientific: Highly sensitive and reliable analysis of distillate products as per ASTM Method D8110 using single quadrupole ICP-MS</strong></h4><ul><li>Application note</li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/paper/28389"><strong>Full PDF for download</strong></a></li></ul><p>The goal of this application note is to demonstrate the performance of an analytical method for routine analysis of typical samples relevant to the petrochemical industry, including starting materials such as crude oil but also products such as naphtha, with different boiling ranges using single quadrupole ICP-MS following the guidelines provided in ASTM Method D8110 Standard Test Method for Elemental Analysis of Distillate Products by Inductively Coupled Plasma Mass Spectrometry (ICP-MS).</p><h5><strong>Conclusions</strong></h5><p>The results obtained from the experiments described in this application note demonstrate the following:</p><ul><li>The proposed method and instrument set-up for elemental analysis of different petroleum products using the iCAP MSX ICP-MS represents a viable solution for laboratories performing oil and refinery product testing.</li><li>The combination of the sample introduction system together with a uniquely robust plasma generation system and a powerful CRC allows for sensitive analysis and comprehensive interference removal for all elements commonly analyzed in the industry. A common sample preparation method encompassing simple dilution of any products with either higher viscosity or lower boiling point in PremiSolv offers complete flexibility for the analysis of a variety of based petroleum sample matrices.</li><li>The use of KED with helium provided effective for removal of polyatomic interferences commonly observed in such challenging matrices, as was demonstrated by the detection limits and blank equivalent concentrations (BECs) achieved.</li><li>The method therefore allows the accurate and precise determination of a total of 28 elements in different kinds of distillate products, as was demonstrated by the results obtained in the spike recovery test.</li><li>If needed, other reactive gases can be used in a multi-mode analysis performed during a single aspiration of a sample, including alternative cell gases such as hydrogen. Thanks to the fast gas switching in the QCell CRC, the added time for switching cell gases is often negligible for the overall analysis time per sample.</li></ul><p>Taken together, the results obtained demonstrate that the proposed analytical method can be used in routine laboratories to achieve high-throughput, robust, and reliable analytical results with minimum downtime of the system.</p><h4><strong>3. Agilent Technologies: Improved Lab Efficiency with the Agilent 18-Cell Changer Accessory</strong></h4><ul><li>Application note</li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/paper/26590"><strong>Full PDF for download</strong></a></li></ul><p>Evaluation of an Agilent Cary 60 UV-Vis spectrophotometer workflow using the 18-cell changer accessory</p><h5><strong>Introduction</strong></h5><p>In laboratory settings, time is of the essence. The speed at which any experiment can be conducted is important, and any advantages that can improve speed are critical. It is equally important that analytical workflows are optimized for maximum instrument use and minimal operator interaction.</p><p>The Agilent Cary 60 UV-Vis spectrophotometer is a flexible, powerful, and reliable UV-Vis system, ideal for routine analysis. To further improve workflow efficiency, the Cary 60 UV-Vis can be equipped with the Agilent 18-cell changer accessory. The 18-cell changer can measure up to 18 cuvettes in sequence, without any user interaction.</p><p>This technical overview compares a Cary 60 UV-Vis workflow using the 18-cell changer accessory versus a single-cell holder accessory to evaluate differences in terms of analysis time, data quality, user interaction, ease of use, and efficiency.</p><h5><strong>Conclusion</strong></h5><p>In summary, the Agilent 18-cell changer accessory for the Agilent Cary 60 UV-Vis spectrophotometer provides a range of benefits to laboratories and technicians alike. Compared to a single-cell holder, it dramatically increases efficiency by reducing the time taken to complete experiments and limiting the need for operator interaction, all without compromising the quality of results.</p><h4><strong>4. Shimadzu: Sensitivity Evaluation and Example Analysis of Microscopic Targets with Thermoelectrically Cooled MCT Detector</strong></h4><ul><li>Application note</li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/paper/28644"><strong>Full PDF for download</strong></a></li></ul><h5><strong>User Benefits</strong></h5><ul><li>A thermoelectrically cooled MCT detector can measure microscopic targets down to 25 μm in size without needing liquid nitrogen.</li><li>An MCT detector is compatible with transmission, reflection, and ATR method for analyzing a range of sample types.</li><li>For targets smaller than 25 μm, the standard T2SL detector can measure targets down to 10 μm in size with good sensitivity.</li></ul><h5><strong>Introduction</strong></h5><p>Infrared spectroscopy is extremely useful for qualitative analysis of organic compounds and some inorganic compounds. Infrared microscopy can be used for spectroscopic analysis of microscopic targets that are otherwise difficult to analyze. The AIMsight Infrared Microscope and the infrared mode of the AIRsight Infrared/Raman Microscope are equipped as standard with the T2SL detector, which can analyze microscopic targets down to 10 μm in size if it is cooled with liquid nitrogen. However, the difficulties associated with procuring and handling liquid nitrogen mean there is increasing demand for infrared spectroscopic analysis of microscopic targets without using liquid nitrogen.</p><p>The thermoelectrically cooled (TEC) MCT detector is a new optional detector in Shimadzu’s product lineup that can analyze microscopic targets down to 25 μm in size without liquid nitrogen. This Application News compares this new detector with existing detectors and presents two example analyses of microscopic targets using the new detector.</p><h5><strong>Conclusion</strong></h5><p>This Application News compares the sensitivity of the new TEC MCT detector with existing detectors and presents two example analyses performed using the TEC MCT detector. The comparisons show the TEC MCT detector, which operates without liquid nitrogen, can measure targets as small as 25 μm with good sensitivity, and it is compatible with reflection and ATR spectroscopy as well as transmission spectroscopy for analysis of a range of sample types.</p><p>The T2SL detector, which requires liquid nitrogen, is recommended when analyzing targets smaller than 25 μm or when using fewer scans to shorten the analysis time. However, the minimum target size for infrared spectroscopic analysis with the T2SL detector is 10 μm, so targets smaller than 10 μm, Raman spectroscopy with the AIRsight infrared/Raman microscope should be used.</p>

News from LabRulezICPMS Library - Week 3, 2025

<p><strong>In the week from January 20, the following webinars await you in the field of atomic and molecular spectroscopy and spectrometry</strong></p><blockquote><p><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinars"><strong>👉 DETAILS AND REGISTRATION IN THE WEBINARS SECTION</strong></a></p><p><strong>👉 Search and filter in the largest global database</strong> with over <strong>4 000 GC, LC, MS and spectroscopy webinars</strong>.</p></blockquote><h5><strong>1. Anton Paar: Fundamentals of Scratch</strong></h5><div><div><ul><li><div>Tu, 21.1.2025 20:00 CET</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/4449">Registration</a></div></li></ul></div><p>This webinar provides a thorough introduction to the theory and practice of instrumented scratch testing, a critical method for evaluating the mechanical properties of materials under stress.</p></div><h5><strong>2.&nbsp;Mettler-Toledo: Advanced Inspection of Canned Goods with X-ray Inspection</strong></h5><div><div><ul><li><div>We, 22.1.2025 09:00 CET</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/4658">Registration</a></div></li></ul></div><p>Join our webinar to discover the wide range of benefits that x-ray inspection offers canned applications - including advanced detection capabilities and integrity and completeness checks.</p></div><h5><strong>3.&nbsp;Bruker: Nanoscale Chemical Characterization of Semiconductor Materials and Devices using Photothermal AFM-IR</strong></h5><div><div><ul><li><div>We, 22.1.2025 17:00 CET</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/4681">Registration</a></div></li></ul></div><p>In this webinar, Bruker nanoscale IR spectroscopy experts show how photothermal AFM-IR can identify the local chemistry of defects.</p></div><h5><strong>4.&nbsp;Agilent Technologies: Using LDIR for Advanced Microplastics Characterization</strong></h5><div><div><ul><li><div>Th, 23.1.2025 09:00 CET</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/4683">Registration</a></div></li></ul></div><p>This session will highlight the advanced features of LDIR technology and its critical applications in analyzing microplastics within various matrices.</p></div><h5><strong>5.&nbsp;LECO: Optimization of Combustion Methods for Determination of Low-Level Nitrogen-Protein in Food</strong></h5><div><div><ul><li><div>Th, 23.1.2025 16:00 CET</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/4686">Registration</a></div></li></ul></div><p>In this webinar, Lloyd Allen, Ph.D., LECO's Director of the Technical Services Laboratory, will share practical insights on overcoming challenges using advanced combustion instruments.</p></div><h5><strong>6.&nbsp;Agilent Technologies: Different Cones / Nebulizers / Sample Introduction Systems .. Where and When to Use them</strong></h5><div><div><ul><li><div>Th, 23.1.2025 20:00 CET</div></li><li><div><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/4546">Registration</a></div></li></ul></div><p>Different Cones / Nebulizers / Sample Introduction Systems .. Where and When to Use them</p></div>

Webinars LabRulezICPMS Week 4/2025

<p><strong>Bohumil Kolář applies artificial intelligence in places where ordinary people can hardly imagine it. We talked about how AI makes work easier, how construction kit Mercur continues to inspire a hundred years after its creation, and beer cups whose meaning will blow your mind.</strong></p><p>I'm taking pictures of Bohumil with the computer. "<i>And now I'm going to take a picture of you with neural networks</i>," I say mischievously. "<i>Well, we have some graphic simulation, so I can send it to you</i>," Bohumil replies with hesitation. I can see that my sense of humor is off, so I'm getting insecure with the conversation. ChatGPT is now an integral part of my life, but what's behind it, I don't know. And Bohumil knows, he's an AI expert.</p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/TUL_CXI_Bohumil_Kolar_5cdb8ef8d0.jpg" alt="TUL CXI: Bohumil Kolář" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_TUL_CXI_Bohumil_Kolar_5cdb8ef8d0.jpg 231w," sizes="100vw" width="800" height="540"></p><h5><strong>Sometimes I'm lazy</strong></h5><p>And what does Bohumil use ChatGPT for? "<i>Sometimes I'm just lazy</i>," Bohumil admits. "<i>The AI saves me hours of reading</i>," he says with a guilty smile. "<i>Sometimes I copy a long text into ChatGPT and ask it to summarize it in two paragraphs. Why? Because I don't always have the desire or time to read anything longer than two pages</i>," he explains candidly.</p><p>Bohumil found out about the AI Specialist position at CXI TUL when he was looking for a job after school. "<i>For example, I was offered a job developing a cable car control system, which is not interesting for me. Then I found an offer from CXI TUL and I'm happy, I often learn new things. I enjoy challenges. For example, I am working on an AI application for laser calibration</i>," he shrugs. The aforementioned laser has many applications, for example from eye surgery, through brute force cutting to space research and defense systems.</p><h5><strong>It started with Mercur</strong></h5><p>Bohumil was a fan of the construction kit Merkur as a kid, but he was missing something to get the kit moving. So he became interested in electrical engineering. He soon discovered that there was always a need for a man to program everything. "<i>I'm not really a programmer, I've always been attracted to the interdisciplinary field, the connection with electrical engineering. Now, for example, I'm tackling business efficiency with artificial intelligence in the European Digital Innovation Hub, </i><a target="_blank" rel="noopener noreferrer" href="https://www.edih-northeast.cz/en/home/"><i>EDIH</i></a>."</p><h5><strong>Real problems, practical solutions</strong></h5><p>Businesses from across the spectrum of industries turn to Bohumil directly or attend training sessions where he shows them the possibilities of AI to streamline operations. "<i>For example, Škoda approached us about vibrodiagnostics. The brief was to see if we could predict when an engine would break down. My job was to teach AI to recognize the vibration of a balanced engine and detect deflections such as bearing float, unbalance, and so on. Based on this data, they can prevent failures and maintain production quality,</i>" Bohumil recounts.</p><h5><strong>Image analysis of wastewater</strong></h5><p>One of the most interesting contracts is the detection of problems at wastewater treatment plants. "<i>My job is to teach the program to recognize what a poorly working treatment plant looks like. For example, foaming water means an overgrowth of microorganisms. Color changes can indicate a different type of problem. Camera detection is fast and efficient, and you don't have to physically go around to all the treatment plants</i>," he says.</p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/TUL_CXI_Bohumil_Kolar_Umela_inteligence_otevira_nove_pracovni_moznosti_5386b28764.jpg" alt="TUL CXI: Bohumil Kolář (Artificial intelligence opens up new job opportunities)" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_TUL_CXI_Bohumil_Kolar_Umela_inteligence_otevira_nove_pracovni_moznosti_5386b28764.jpg 117w," sizes="100vw" width="1500" height="2000"></p><h5><strong>AI and Beer cups</strong></h5><p>And what does Bohumil have on his desk besides his computer? "<i>Lots of beer cups</i>," he laughs. One of his apps detects whether you have an honest pint in front of you or under measurement.</p><p>The audience immediately thinks: nice, but what is it good for? "<i>The same algorithm can detect a tank and guide a missile. Maybe in Ukraine,</i>" Bohumil answered laconically. It shows that even a seemingly innocent AI application can be a weapon.</p><h5><strong>Revolution</strong></h5><p>The rapid development of artificial intelligence is a challenge for Bohumil. "<i>The pace at which AI is growing is insane,</i>" he says. "<i>New algorithms and technologies are being created every day. Sometimes I must understand how a certain technology works, only to find out a year later that it's already outdated. The world's largest organizations are rapidly pushing the boundaries of AI. Guessing the direction of development and keeping track is a big challenge."</i></p><h5><strong>AI gives work</strong></h5><p>From engineering to natural sciences, Bohumil sees no limits to artificial intelligence. "<i>The only problem is the lack of data to train the models.</i>" Many people argue that AI is taking jobs. Bohumil sees it differently. “<i>Automation opens up opportunities for more work.</i>"</p><p>It is important to show that AI is a tool. "<i>It is not a threat. It depends on how we use it,</i>" concludes Bohumil.</p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/TUL_CXI_Bohumil_Kolar_Umela_inteligence_otevira_nove_pracovni_moznosti_2_e943a453a0.jpg" alt="TUL CXI: Bohumil Kolář (Artificial intelligence opens up new job opportunities)" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_TUL_CXI_Bohumil_Kolar_Umela_inteligence_otevira_nove_pracovni_moznosti_2_e943a453a0.jpg 117w," sizes="100vw" width="1500" height="2000"></p>

Bohumil Kolář: Artificial intelligence opens up new job opportunities

<p><strong>Our Library never stops expanding. What are the most recent contributions to LabRulezICPMS Library in the week of 20th January 2025? Check out new documents from the field of spectroscopy/spectrometry and related techniques!</strong></p><blockquote><p><span style="font-size:20px;">👉 </span><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/library"><span style="font-size:20px;"><strong>SEARCH THE LARGEST REPOSITORY OF DOCUMENTS ABOUT SPECTROSCOPY/SPECTROMETRY RELATED TECHNIQUES</strong></span></a></p></blockquote><blockquote><p><strong>👉 Need info about different analytical techniques?</strong> Peek into <a target="_blank" rel="noopener noreferrer" href="https://lcms.labrulez.com/library"><strong>LabRulezLCMS</strong></a> or <a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/library"><strong>LabRulezGCMS</strong></a> libraries.</p></blockquote><p>This week we bring you applications by <strong>Shimadzu, Agilent Technologies </strong>and<strong> Thermo Fisher Scientific!</strong></p><h4><strong>1. Shimadzu: TOC Analysis for Evaluation of Plastics and Other Organic Materials in Contact with Drinking Water</strong></h4><ul><li>Application note</li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/paper/28646"><strong>Full PDF for download</strong></a></li></ul><h5><strong>User Benefits</strong></h5><ul><li>TOC analysis helps ensure compliance with EU regulations for materials in contact with drinking water, protecting public health and maintaining high water quality standards.</li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/library?instrumentationItems=103&amp;mainauthorItems=1&amp;search=TOC-L+CPH"><strong>TOC-L </strong></a>supports a comprehensive analysis capable of testing a wide range of components, thus helping to obtain conformity certification for the hygienic suitability of products in contact with drinking water.</li></ul><h5><strong>Introduction</strong></h5><p>Ensuring the purity of drinking water during production and distribution is a critical requirement. Quality standards are defined by the European Union in the Drinking Water Directive (EU) 2020/2184, where Article 11 specifically addresses materials that come into contact with water (Table 1) . These materials must not adversely affect human health, alter the taste, color or odor of the water, contribute to microbial growth or release significant quantities of contaminants. In essence, no extractable substances from these materials should contaminate drinking water. Therefore, the technical and hygienic suitability of products in contact with drinking water must be verified by laboratory tests.</p><p>Article 11 (EU) of 2020/2184 is essentially based on the "4 Member States Initiative" (4MSI) common approach for organic materials. One guideline that has dealt with this topic to date is the KTW guideline (German for Plastics - Drinking Water) from the German Federal Environment Agency. It was used for the hygienic assessment of organic materials in contact with<br>drinking water and describes the requirements that plastics must meet in this context. As guidelines tend to be of a recommendatory nature, the EU has obliged its member states to specifically regulate the requirements for materials in contact with drinking water. Accordingly, the Federal Environment Agency published the KTW-BWGL (Plastics Drinking Water Assessment Guideline) in March 2019. It officially replaced the previous recommendations of the KTW guideline.</p><h4><strong>2.&nbsp;Agilent Technologies: Agilent 8800 ICP-QQQ Upgrades</strong></h4><ul><li>Other</li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/paper/28650"><strong>Full PDF for download</strong></a></li></ul><p>Upgrading your 8800 to an Agilent 8900 provides a seamless transition, as the new instrument can replace your existing 8800 with minimal disruption to your lab’s operations:</p><ul><li>Existing laboratory services – power, exhaust vent, and gas supplies – will still be suitable</li><li>Major peripherals such as the ASX and SPS 4 autosamplers and water chiller/recirculator can still be used</li><li>Many consumables (torches, sampling cones, tubing) are compatible</li><li>Upgrading also gives you access to the latest in ICP-QQQ technology as well as the upgraded UHMI High Matrix Introduction system<sup>1</sup>.</li></ul><h5><strong>Upgrading your Agilent 8800 ICP-QQQ</strong></h5><p>For a limited time, Agilent is offering 8800 Series ICP-QQQ users the opportunity to upgrade their ICP-QQQ instrumentation to the latest, high-performance, Agilent triple quadrupole ICP-QQQ. The Agilent 8900 is the ideal replacement for your 8800, as it provides continuity of analytical capability but with even better performance. The 8900 is also compatible with your existing bench space and lab services.</p><p>With the 8900, there is no need to compromise the unmatched matrix tolerance, helium, and unparalleled reaction cell mode performance and wide detector dynamic range that made the 8800 such a remarkable success.</p><h4><strong>3.&nbsp;Thermo Fisher Scientific: A comprehensive workflow for beverage analysis using inductively coupled plasma mass spectrometry (ICP-MS)</strong></h4><ul><li>Application note</li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/paper/28429"><strong>Full PDF for download</strong></a></li></ul><p>This application note will highlight a complete and comprehensive workflow for the analysis of nutrients and toxic trace elements in different types of beverages. Samples were digested using a microwave system prior to analysis using triple quadrupole ICP-MS for analysis.</p><h5><strong>Introduction</strong></h5><p>Trace metals analysis in beverages plays a crucial role in ensuring the safety, quality, and compliance of these products, helping to protect consumer health and maintain the reputation of beverage manufacturers.</p><p>Trace metals can enter beverages through various sources, starting from their natural occurrence in the ingredients, water used in production, or through processing equipment, packaging materials, etc. The presence of these metals in excessive amounts can pose potential health risks to consumers, making it necessary to monitor and control their levels. Typical analytes include, but are not limited to, arsenic, cadmium, lead, mercury, and copper. The analysis is essential to ensure the safety and quality of beverages consumed by humans.</p><p>Regulatory bodies, such as the World Health Organization (WHO) and the Food and Drug Administration (FDA), have established guidelines and maximum allowable limits for trace metals in beverages to ensure consumer safety. Manufacturers and regulatory authorities rely on the analysis to verify compliance with these regulations and to maintain the quality and integrity of beverages in the market.</p><p>It is important to note that concentration limits can vary depending on the specific beverage type and the intended consumer population (e.g., infants, children, adults). Furthermore, applicable regulations and guidelines are regularly updated, so it is crucial for beverage manufacturers to stay informed about the latest requirements in their respective markets to ensure compliance.</p><p>On the other hand, there are several essential inorganic elements that are vital for various physiological processes in the body. Nutrients such as calcium, phosphorous, sodium, potassium, magnesium, iron, and zinc serve essential roles in various physiological processes within the human body and provide the building blocks for growth, development, and maintenance of tissues and organs. These elements therefore play crucial roles in maintaining overall health and supporting various bodily functions.</p><p>This application note demonstrates a workflow for highly reproducible sample preparation combined with sensitive and robust analysis for a wide variety of beverages. The proposed workflow allowed accurate determination of both essential nutrients and potentially toxic trace metals without any compromise and can be implemented, for example, in analytical testing laboratories performing the analysis on behalf of manufacturers or regulatory authorities.</p><h5><strong>Conclusion</strong></h5><p>This workflow, combining sample preparation using microwave assisted digestion and analysis using the <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/products/1488"><strong>iCAP MTX ICP-MS</strong></a>, allows the determination of nutrient composition of fruit juices and processed beverages as required by the food labeling regulations and detection of any contaminants such as toxic elements present in the beverages.</p><p>The analytical method was proven to provide accurate and precise results and can provide reliable performance over long analysis sequences, ensuring productivity in an applied testing laboratory. Based on the automatic and constant 5-times dilution of all samples, there are no matrix effects that would lead to unwanted interruptions of the analysis due to QC failures. Samples can be placed on the autosampler after completing preparation; no additional dilution is required. All types of interferences (polyatomic as well as isobaric interference, including doubly charged ions) are effectively suppressed with either helium collision gas or by using oxygen as a reactive gas in triple quadrupole mode. The instrument method could be easily set up thanks to the Reaction Finder method development assistant for <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/products/1489"><strong>Qtegra ISDS Software</strong></a>.</p>

News from LabRulezICPMS Library - Week 4, 2025

Osobnosti

Article

Product

Events

Webinars

Application

Academy

Video

Poster

Scientists

Plastics

Environment

Food

Water

Health

Presentation

Scientific article

Interview

Toxicology

Popularization

Science and research

Software

Covid-19

Career

Laboratories

Various

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News from LabRulezICPMS Library - Week 4, 2025

Bohumil Kolář: Artificial intelligence opens up new job opportunities

Webinars LabRulezICPMS Week 4/2025

People of Brnoregion Microscopy: Jiří Nováček (CEITEC MUNI)

News from LabRulezICPMS Library - Week 3, 2025

Webinars LabRulezICPMS Week 3/2025

The memory of Josef Dadok lives on at CEITEC through cutting-edge research in spectroscopy

News from LabRulezICPMS Library - Week 2, 2025

Webinars LabRulezICPMS Week 2/2025 + TOP 10 in 2024

Revolutionary spectrometer will help scientists understand protein structure and design new drugs

Upcoming events

LECO Training Course CS-744/844 Series

42nd Informal Meeting on Mass Spectrometry

SETAC Europe 36th Annual Meeting

Webinars

TOC Determination in Soil and Waste

Time to Go PRO: Discover the future of ICP-OES analysis

Cement Clinker Preparation and Microscopic Examination