<h4>A comprehensive analysis of renewable fuel testing technologies, automation, and ISO-compliant proximate analysis</h4>The growing demand for renewable energy has increased the importance of accurate biofuel characterization. Biomass feedstocks and finished fuels must be carefully analyzed to ensure quality, efficiency, and compliance with international standards. LECO analytical instrumentation supports this work through automated and highly reliable analytical technologies.<img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/TGA_801_Termogravimetricka_analyza_vlhkosti_popela_tekavych_latek_a_ztraty_zihanim_b73c4cf493.jpg" alt="LECO: Advancing Biofuel Characterization with LECO Analytical Instrumentation: LECO’s TGA801, used for automated biofuel analysis." srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_TGA_801_Termogravimetricka_analyza_vlhkosti_popela_tekavych_latek_a_ztraty_zihanim_b73c4cf493.jpg 245w," sizes="100vw" width="1164" height="435"><h3>Automated Proximate Analysis with LECO’s TGA801</h3>The<a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/products/1877"> LECO TGA801 thermogravimetric analyzer </a>is designed for automated determination of moisture, volatile matter, and ash content in solid fuels. The system can analyze up to 19 samples simultaneously and combine all three parameters into one automated run, improving efficiency and reproducibility.<img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/LECO_Advancing_Biofuel_Characterization_with_LECO_Analytical_Instrumentation_31e96f1c96.jpg" alt="LECO Advancing Biofuel Characterization with LECO Analytical Instrumentation: TGA801 system with ceramic turntable and crucibles for ISO 18123 volatile matter determination." srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_LECO_Advancing_Biofuel_Characterization_with_LECO_Analytical_Instrumentation_31e96f1c96.jpg 235w," sizes="100vw" width="860" height="573"><h3>Comparison with ISO Reference Methods</h3>To validate the performance of the automated TGA801 system, comparative studies were conducted using internationally recognized ISO reference methods. Moisture determination was compared with ISO 18134, ash content with ISO 18122, and volatile matter with ISO 18123. These standards prescribe specific temperatures and analytical procedures, but also permit automated systems if equivalent performance can be demonstrated.The comparison included a broad range of materials such as wood pellets, peat, coal, plastics, and waste-derived fuels. Moisture and ash results generated by the TGA801 showed extremely close agreement with the manual ISO procedures. This strong correlation confirms that automated thermogravimetric analysis can provide the same reliability as conventional methods while greatly increasing throughput and reducing labor requirements.<img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/LECO_Advancing_Biofuel_Characterization_with_LECO_Analytical_Instrumentation_2_3887128788.jpg" alt="LECO: Advancing Biofuel Characterization with LECO Analytical Instrumentation: ISO method crucibles for manual volatile determination." srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_LECO_Advancing_Biofuel_Characterization_with_LECO_Analytical_Instrumentation_2_3887128788.jpg 172w," sizes="100vw" width="1264" height="1145"><h3>Volatile Matter Correlation Results</h3>For volatile matter analysis, both ISO and TGA procedures measure mass loss during a fixed period at 900 °C. The TGA method introduces an additional heating ramp from the moisture determination step at approximately 105 °C to the higher volatile matter temperature. Despite this procedural difference, the resulting data demonstrated excellent agreement.Testing performed on wood pellets showed a strong linear relationship between the ISO and TGA methods with an R² value of approximately 0.94. The maximum deviation observed was only 1.06%, while the average difference between methods was approximately 0.1%. These results confirm the ability of the TGA801 to produce highly accurate volatile matter measurements across a variety of biomass and fuel matrices.<img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/LECO_Advancing_Biofuel_Characterization_with_LECO_Analytical_Instrumentation_2_40f7189cef.jpg" alt="LECO Advancing Biofuel Characterization with LECO Analytical Instrumentation: Correlation and comparative data between ISO methods and LECO TGA analysis." srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_LECO_Advancing_Biofuel_Characterization_with_LECO_Analytical_Instrumentation_2_40f7189cef.jpg 172w," sizes="100vw" width="1065" height="967"><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/LECO_Advancing_Biofuel_Characterization_with_LECO_Analytical_Instrumentation_1_7519e8e646.jpg" alt="LECO Advancing Biofuel Characterization with LECO Analytical Instrumentation: Correlation and comparative data between ISO methods and LECO TGA analysis." srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_LECO_Advancing_Biofuel_Characterization_with_LECO_Analytical_Instrumentation_1_7519e8e646.jpg 228w," sizes="100vw" width="1641" height="1120"><h3>Advantages of Automated Biofuel Analysis</h3><ul><li>High sample throughput with simultaneous multi-sample analysis.</li><li>Fully automated workflows reducing operator involvement.</li><li>Integrated determination of moisture, ash, and volatile matter in one run.</li><li>Excellent reproducibility and data consistency.</li><li>Strong agreement with ISO reference methods without additional calibration.</li><li>Improved data security and laboratory efficiency.</li><li>Suitable for research laboratories, industrial quality control, and fuel certification.</li></ul><h3>Automate Your Lab Today</h3>LECO analytical instrumentation provides a comprehensive solution for modern biofuel characterization. From calorific value determination and elemental composition analysis to ash fusibility and automated proximate analysis, these technologies support both scientific research and industrial production with fast, reliable, and reproducible results. The TGA801 demonstrates how automation can significantly improve laboratory efficiency while maintaining full compliance with ISO reference methods. By integrating moisture, ash, and volatile matter analysis into a single automated workflow, the system reduces labor requirements, increases throughput, and enhances data quality. As renewable energy continues to expand globally, advanced analytical systems will remain essential for ensuring fuel quality, supporting regulatory compliance, and driving innovation in sustainable energy technologies. <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/products/1877">Explore the features of the LECO TGA801 today.</a>

Advancing Biofuel Characterization with LECO Analytical Instrumentation

Researchers&nbsp;Tereza Nešporová and Jaroslava Večerková from Brno's RECETOX explain why failures are also a valuable part of gaining knowledge, how they study the effects of chemical substances on the hormonal system, and why they apply their professional insights to their everyday lives.<h5>How did you get involved in research at RECETOX?&nbsp;</h5>Jaroslava: I actually joined RECETOX by chance during my follow-up Master's studies in Environmental Chemistry, back when Professor Holoubek was still leading the institute. I wrote my thesis under Klára Hilscherová and simply stayed here ever since, except for a break during maternity leave. I have been part of her team the whole time, focusing on endocrine disruptors.&nbsp;What has changed over the years is the focus of our research. We used to study surface waters, particularly the presence of substances with endocrine-disrupting potential and their effects on organisms. Today, the research has shifted more toward humans and the interactions between chemical substances and the endocrine system.&nbsp;Tereza: I came from a completely different field. I studied molecular biology and worked on chronic lymphocytic leukemia for my Master's thesis at CEITEC. I used genetic engineering methods such as CRISPR/Cas9 for gene editing—activating, suppressing, or completely removing genes.&nbsp;At the time, Klára Hilscherová’s group needed to create cellular models with increased production of deiodinase enzymes, which I still work on today. I had heard only positive things about the team, and when I finished my Master's degree, I wanted to move beyond my original field. The connection between hormones and neurodevelopment attracted me, and RECETOX became the obvious choice.&nbsp;<h5>So you are in the same research team. How do you collaborate?&nbsp;</h5>Tereza: We sit in the same office. And that’s probably the main thing (laughs).&nbsp;Jaroslava: We discuss things a lot. Some mechanisms repeat across experiments, so we talk about how each of us evaluates data and why. We inspire each other, even though we do not directly collaborate on the same laboratory work.&nbsp;<h5>How does your work differ?&nbsp;</h5>Tereza: Our team is highly interconnected. We all work on developing assays for detecting endocrine-disrupting substances, specifically those affecting thyroid hormones. However, each of us focuses on a different part of the system.&nbsp;I focus on deiodinase enzymes, which regulate the activation and deactivation of hormones. Recently, I have been spending more time analyzing data and designing experiments than working directly in the laboratory.&nbsp;Jaroslava: Within the team, I mainly participate in testing different types of samples—from individual chemicals and mixtures to real environmental samples such as household dust—using the assays mentioned above.&nbsp;It is important to note that chemicals can affect the hormonal system at different levels. They can bind to or block nuclear receptors, affect hormone transport in the bloodstream, or interfere with hormone metabolism. In the past, only one part of this process was monitored. Today, we aim to cover the full spectrum of these interactions.&nbsp;Tereza: And that is crucial. A substance may appear negative in one test, yet affect another part of the system, producing a significant impact on the organism. That is why current research focuses on the entire range of possible mechanisms.&nbsp;<h5>Why did you choose endocrine disruptors as your research topic?&nbsp;</h5>Jaroslava: For me, it was more or less a coincidence while choosing my thesis topic. But it turned out to be a fascinating area, so I stayed with it.&nbsp;Tereza: I had been interested in it for a long time. I also like that our work has a concrete outcome—we develop tests that can realistically be used in decision-making regarding the safety of chemical substances. Compared to my previous research, I feel this work has a much more direct application.&nbsp;<h5>What about your PhD studies?&nbsp;</h5>Jaroslava: My PhD studies are currently on hold. After maternity leave, I returned as a laboratory technician, and my project work gradually shifted away from my original doctoral topic.&nbsp;Tereza: I am currently in the fourth year of my PhD studies. I also completed a research stay in Germany, where I learned to work with neuronal cells.&nbsp;As part of my studies, I focus mainly on deiodinases—the enzymes that act as the “on and off switches” of thyroid hormones. We are developing a test that can measure the effects of chemical substances on their activity.&nbsp;In addition, we are now studying how these substances affect neurons and their development, because proper thyroid hormone levels are crucial for nervous system development.&nbsp;<h5>What is the most challenging aspect of laboratory work?&nbsp;</h5>Tereza: Probably unpredictability. Cells do not always grow as expected, instruments have their bad days, and human error also plays a role. The important thing is to document all mistakes and complications and learn from them.&nbsp;Jaroslava: I agree with Tereza. The biggest challenge is unpredictability. Cells are living systems and do not always behave the same way.&nbsp;<h5>Can a career in science be combined with parenthood?&nbsp;</h5>Jaroslava: At RECETOX, definitely. There is a great deal of flexibility, and managers are very supportive. When necessary, it is possible to work from home. We help each other a lot within the team.&nbsp;Tereza: It also depends on the type of work and whether it can be planned according to your needs. Our team collaborates closely and tries to help one another whenever necessary. That is key. And when needed, data analysis and manuscript writing can also be done from home.&nbsp;<h5>Is your work more routine or highly varied?&nbsp;</h5>Jaroslava: Very varied. Laboratory work alternates with computer-based work. We are constantly learning new things. It is definitely not repetitive or boring, and that is what I enjoy about it.&nbsp;Tereza: The only routine in my work is taking care of cell cultures. Otherwise, the work is constantly changing. That is also what I enjoy most about it.&nbsp;<h5>What are the biggest challenges in your work?&nbsp;</h5>Jaroslava: Data evaluation. Measuring something is one thing; evaluating and interpreting it correctly is another.&nbsp;Tereza: Implementing new methods. And also those moments when you do everything correctly according to a published protocol, yet the results still do not match expectations.&nbsp;In science, you have to learn to accept that not everything works the first time. The important thing is not to give up, to continue optimizing, and to keep hoping for success.&nbsp;<h5>What role should open science play?&nbsp;</h5>Tereza: A huge one. If we had access to detailed protocols and original datasets, it would save enormous amounts of time and money during the implementation and optimization of new methods. Scientific papers often omit details that are actually critical for experimental success.&nbsp;Jaroslava: It is also important to share failures. A negative result is still a result, and it can provide valuable information.&nbsp;<h5>You are both mothers. Does your work influence your personal lives?&nbsp;</h5>Jaroslava: Absolutely. For example, we pay close attention to washing fruit because of chemical treatments. I encourage my children to think about what they consume, what it contains, and where it comes from. We try to avoid plastics and consistently separate waste.&nbsp;Tereza: Definitely. Even before having a child, I paid close attention to the composition of cosmetics, food, and other products. After becoming a parent, my caution multiplied.&nbsp;I was especially careful during pregnancy because a developing organism is most sensitive to harmful substances. Sometimes relatives raise their eyebrows at this, but when we have information firsthand, we cannot simply ignore it.&nbsp;Jaroslava: We also pay attention to toys, clothing, and materials used in the home. It is a kind of professional deformation (laughs).&nbsp;<h5>How can your research contribute from a broader perspective? How can others build upon it?&nbsp;</h5>Jaroslava: We are gradually optimizing methods that may eventually be used routinely. That is probably our greatest contribution.&nbsp;Tereza: Yes, our methods could help identify undesirable effects of substances before they reach the market, potentially leading to regulation of their production.&nbsp;<h5>Would you like to continue working on this topic in the future?&nbsp;</h5>Jaroslava Večerková: The topic of endocrine disruption is extremely interesting and very broad. The direction of research may change depending on current projects, but I would like to remain part of the team.&nbsp;Tereza Nešporová: I am very interested in uncovering how substances affect human health, and I believe I will want to continue working in this area. I like how dynamic the research is and that it has direct practical applications. I do not mind change, but I am happy within this team and would like to stay. We work together as a well-coordinated group.&nbsp;

Researchers Tereza Nešporová and Jaroslava Večerková: In science, we must learn to work with failure

Our Library never stops expanding. What are the most recent contributions to LabRulezICPMS Library in the week of 6th July 2026? Check out new documents from the field of spectroscopy/spectrometry and related techniques!<blockquote>👉 <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/library">SEARCH THE LARGEST REPOSITORY OF DOCUMENTS ABOUT SPECTROSCOPY/SPECTROMETRY RELATED TECHNIQUES</a></blockquote><blockquote>👉 Need info about different analytical techniques? Peek into <a target="_blank" rel="noopener noreferrer" href="https://lcms.labrulez.com/library">LabRulezLCMS</a> or <a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/library">LabRulezGCMS</a> libraries.</blockquote>This week we bring you brochure by Agilent Technologies, application note by Shimadzu and other document by Thermo Fisher Scientific!<h3>1. Agilent Technologies: The Easiest Smart Decision You Can Make - The Agilent 9500 ICP-MS</h3><ul><li>Brochure</li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/labrulez-bucket-strapi-h3hsga3/br_9500_icp_ms_5994_9160en_agilent_240554d484.pdf">Full PDF for download</a></li></ul>The brochure presents the <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/library?mainauthorItems=10&amp;search=9500">Agilent 9500 ICP-MS</a> as an ICP-QQQ system designed to bring triple quadrupole performance into routine laboratories without adding unnecessary complexity. It addresses common ICP-MS challenges such as spectral interferences, complex matrices, method development, re-runs, and the limitations of single quadrupole ICP-MS. The 9500 is positioned as a system that delivers reliable, interference-free trace element data while simplifying operation, method setup, and troubleshooting.A central feature of the system is Agilent’s proprietary Dual-Cell System (DCS), which combines Advanced Helium Mode (AHM) and Air mode. AHM replaces multiple traditional tune modes with one streamlined mode, helping reduce acquisition time by more than 33% while improving sensitivity, especially for low-mass elements. Air mode uses ambient air for oxygen mass-shift reactions, enabling effective removal of difficult on-mass interferences without the need for additional oxygen cylinders or related safety infrastructure.The brochure also highlights the system’s practical design improvements. These include Easy-fit sample introduction, automatic gas connections and torch alignment, improved access to the spray chamber, torch, cones, and peristaltic pump, reduced power consumption, lower exhaust flow, enhanced corrosion resistance, and a smaller footprint compared with previous ICP-QQQ systems. The 9500 also supports demanding applications such as high-salinity seawater analysis, rare earth element interference removal, and sub-ppt impurity analysis in high-purity titanium.Software and automation are presented as key parts of the workflow. <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/library?mainauthorItems=10&amp;search=OpenLab+ICP-MS">OpenLab ICP-MS </a>provides method development tools such as Method Advisor, preset methods, batch conversion from existing single quadrupole ICP-MS methods, guided diagnostics, reporting, and IntelliQuant screening. The 9500 can also be integrated with Agilent autosamplers, the AVS MS switching valve, and ADS 2 autodilutor to automate calibration, dilution, analysis, and reporting. Overall, the brochure positions the Agilent 9500 ICP-MS as a more accessible, productive, and future-ready ICP-QQQ platform for laboratories needing reliable results across complex sample types.<h3>2. Shimadzu: Continuous Automatic Measurement of Static Spring Constant and Dynamic Properties before and after Durability Tests on Rubber Vibration Isolators by Combination Test Software</h3><ul><li>Application note</li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/labrulez-bucket-strapi-h3hsga3/an_01_01061_en_7301fb4069.pdf">Full PDF for download</a></li></ul>A rubber vibration isolator is a product designed to prevent or mitigate the transmission of vibration and shock. It is widely used in various fields such as transportation equipment, construction, and industrial machinery.&nbsp;<a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/library?mainauthorItems=1&amp;search=JIS+K+6385">JIS K 6385</a> “Rubber vibration isolators - Test methods” defines several test methods and terms for evaluating the performance of rubber vibration isolators. In order to estimate the fatigue life of rubber vibration isolators, a durability test method is specified in which the rubber vibration isolator is subjected to repeated loads to evaluate the presence of failure, cracks, or changesin properties. It is extremely important to evaluate the durability of rubber vibration isolators because deterioration in their performance can cause noise and instability.&nbsp;Shimadzu’s fatigue and endurance testing machine Servopulser’s Windows Software for 4830 has a function called a combination test, which automatically combines several tests and continuously executesthem. This article introduces an example of continuous automatic measurement of static spring properties and dynamic properties of rubber vibration isolators before and after durability tests, by using a combination test.<h4>Testing Equipment&nbsp;</h4>The EMT-1kNV-50 electromagnetic fatigue and endurance testing machine was used in these tests. Fig. 2 shows a photograph of the testing machine. The electromagnetic actuator with extremely high frequency response enables highly accurate dynamic testing. In these tests, the maximum test frequency was 100 Hz. The EMT series is most suitable for testing at such high frequencies.<h4>Conclusion&nbsp;</h4>A fatigue and endurance testing machine was used to compare the static spring properties and dynamic properties of rubber vibration isolators before and after durability testing based on JIS K 6385. Combination testing software enables continuous and automatic execution of each test, thus reducing work time. The highly responsive EMT series also enables high-frequency testing with amplitudes of 0.05 mm and 100 Hz.<h3>3. Thermo Fisher Scientific: Enhancing Monoclonal Antibody Yield and Quality Through Automated Multi-Component Feedback Control Loops Using the MarqMetrix All-In-One Process Raman Analyzer</h3><ul><li>Other document</li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/labrulez-bucket-strapi-h3hsga3/monitoring_polymer_extrusion_wp1275_en_19f05a5436.pdf">Full PDF for download</a></li></ul>Understanding the structural changes of polymers during the extrusion process is essential for optimizing the manufacturing of extruded products. Extrusion can alter a polymer’s structure and properties in ways that can enhance its performance and functionality. Changes such as the transition from crystalline to amorphous phases or shifts in vibrational modes can be leveraged to tailor the end-polymer’s mechanical, thermal, and optical properties to meet specific application needs.&nbsp;Polymer extrusion is a high-volume manufacturing process where raw plastic materials, such as low-density polyethylene (LDPE) and polylactic acid (PLA), are melted and pushed through a shaped die to create specific and continuous profiles. In twin-screw extruders, this is accomplished using two intermeshing screws and a heating system to increase temperature, shear forces and pressure, in order to efficiently melt and homogenize the polymers. This process allows for the production of a wide range of plastic products with consistent shapes and properties.&nbsp;In addition to polymeric applications, twin-screw extruders are commonly used in pharmaceutical applications for mixing active pharmaceutical ingredients (APIs) with excipients. In battery manufacturing, extruders are used to thoroughly mix anode and cathode materials needed for homogeneous end products. The Thermo Scientific™ Process™ 11 Parallel Twin-Screw Extruder is an ideal tool for processing and compounding various materials in this manner.Vibrational spectroscopic techniques such as Raman spectroscopy are often utilized for off-line evaluation of extrusion products. However, if such techniques can be integrated in line with the extruders, it can facilitate real-time measurements of many qualitative and quantitative aspects of the process.&nbsp;Raman spectroscopy is a technique used to observe vibrational, rotational, and other low-frequency modes in a material. Raman spectroscopy works by shining a monochromatic light source, typically a laser, onto a sample. The light interacts with the molecular vibrations within the sample, causing the light to scatter. Most of the scattered light has the same wavelength as the incident light (Rayleigh scattering), however, a small portion of the scattered light has different wavelengths due to interactions with molecular vibrations. This change in wavelength provides a unique spectral fingerprint of the material, which can be used to identify and characterize the sample’s molecular composition and structure. This data can be translated into quantitative or qualitative information with the use of chemometric modeling techniques such as partial least squares (PLS) regression or principal component analysis (PCA).The <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/products/2233">Thermo Scientific™ MarqMetrix™ All-In-One Process Raman Analyzer</a> allows users to implement Raman spectroscopy directly in line with an extrusion process by using strong and chemically resistant optical probes. MarqMetrix probes can be integrated in line with extruder barrels allowing the continual monitoring of the extrusion process to make quantitative and qualitative decisions in real time.This white paper highlights the integration of the MarqMetrix All-In-One Process Raman Analyzer with the Process 11 Parallel Twin-Screw Extruder to observe polymer processing in real time, directly within the barrel of the extruder. Raman spectroscopy was first used to characterize the differences between the virgin material prior to extrusion, and the same material during extrusion. It was then utilized to indicate when materials had been mixed and then to track the transition from one polymer to another within the extruder system using qualitative chemometric models.&nbsp;The materials used in this study were LDPE and PLA. These materials were chosen due to their popularity in end-products across multiple industries as well as their well-characterized Raman spectra.<h4>Conclusion&nbsp;</h4>The integration of the MarqMetrix All-In-One Process Raman Analyzer with the Process 11 Parallel Twin-Screw Extruder has demonstrated significant benefits for real-time, inline process monitoring in polymer extrusion. This study highlighted the capability of Raman spectroscopy to effectively differentiate between solid and molten states of polymers and provided clear identification of transitions from one polymer to another using PCA models. Such information can be utilized to ensure no cross-contamination during polymer change overs and to ensure the quality of the extruded polymers. This proofof-concept study can be further applied to quantify the composition of the composite polymer materials using PLS models. Additionally, the MarqMetrix All-In-One analyzer can also be integrated mid-barrel to understand the reactive extrusion in real time.&nbsp;Overall, the implementation of Raman spectroscopy into polymer extrusion processes offers a multitude of benefits, ranging from real-time monitoring and quality control to process optimization and cost savings. These advantages make Raman spectroscopy an invaluable tool for enhancing the efficiency and effectiveness of polymer extrusion operations

News from LabRulezICPMS Library - Week 28, 2026

Article

Product

Application

Scientists

RECETOX (Research Centre for Toxic Compounds in the Environment) is an independent department of the Faculty of Science of Masaryk University in Brno, which has been established in 1983. RECETOX is focused on the research and education in cross-cutting area of Environment and Health. It addresses interactions among chemicals, environment, and biological systems, including consequences at local, regional, and global levels.

RECETOX - Centrum pro výzkum toxických látek v prostředí

Everything from the world of analytical chemistry in one place. We connect people in solving their problems. At Labrulez you will find all the necessary information easily, quickly and clearly. Stop searching and start finding.

LabRulez

In 1936, the Laboratory Equipment Company introduced the first rapid carbon determinator for the American iron and steel industry.  Today, almost 80 years later, LECO is recognized globally as a leader in the development of high-quality analytical instrumentation, mass spectrometers, comprehensive two-dimensional chromatography, metallography & optical equipment as well as consumables.

LECO

New Food magazine

Mettler-Toledo

Agilent Technologies

Bruker

Thermo Fisher Scientific

Wiley

From meteorites to pre-solar grains, the study of extra-terrestrial material requires advanced capabilities using multi-scale, multi-modal correlative analysis.
Quantitative mineral identification and crystal orientation using deep-learning enhanced X-ray microscopy generate complete 3D characterization of precious samples.
Electron microscopy techniques focus on maximizing quantitative analysis from microstructural variations to nanoscale trace element analysis.
Attendees will hear about some of the exciting work in extraterrestrial samples, learn about some of the newest analytical techniques that help us to understand the formation of the universe, and how to best study return mission samples that may be no larger than a speck of dust.
<blockquote>
Presenter: Dr. Rich Taylor (Geoscience Applications Development, ZEISS Research Microscopy Solutions - Geoscience)
</blockquote>
<blockquote>
Dr. Rich completed a PhD in Experimental Petrology at the University of Edinburgh in 2009, before moving to Curtin University in Western Australia as a SIMS laboratory specialist. He subsequently held research positions in the School of Earth and Planetary Sciences at Curtin studying geochemistry and geochronology, specialising in imaging and microanalysis. In 2017 he moved to the University of Cambridge to study magnetic inclusions in Earth’s oldest materials using novel microscopy techniques. In 2019 Rich moved to Zeiss based in Cambourne, UK to take on the global Geosciences Applications Development role.
</blockquote>

Wiley: From Deep Space to Deep Learning. State of the Art Imaging of Extraterrestrial Samples

From Deep Space to Deep Learning. State of the Art Imaging of Extraterrestrial Samples

Learn about some of the newest analytical techniques that help us to understand the formation of the universe, and how to best study return mission samples.

State of the Art Imaging of Extraterrestrial Samples

With advancements in battery technology, electricity has become an essential part of modern society, powering a wide array of devices, from smartphones and laptops to electric vehicles (EVs). As we navigate towards a low-carbon economy, storage systems will play a pivotal role in our energy evolution, storing renewable energy and reducing our dependence on fossil fuels. This has resulted in an ever-increasing demand for better batteries, both in terms of production capacity and performance.
As the industry scales up production and recycling efforts, there is a pressing need to enhance battery performance and reduce production costs. Achieving these goals means leveraging the right analytical tools. X-ray analytical techniques like X-ray Diffraction (XRD), X-ray Fluorescence (XRF), and X-ray Microscopy (XRM) are indispensable throughout the entire battery life cycle. They facilitate the development of new cells and components, ensure quality control during manufacturing, and streamline the recycling process. These techniques are essential for optimizing battery performance, enhancing sustainability, and meeting the evolving demands of the energy landscape.
In this live online seminar, our experts will explain what XRD, XRF and XRM can do for you! In lab sessions, we will showcase our devices and provide valuable tips and tricks. Your questions will be answered during our Q&amp;A session.
Agenda (60 min)
<ul>
<li>Introduction</li>
<li>XRD Applications Examples </li>
<li>Lab Session 1: Operando diffraction (XRD)</li>
<li>XRF Applications Examples</li>
<li>Lab Session 2: Precursor analysis (XRF)</li>
<li>XRM Applications Examples </li>
<li>Lab Session 3: Non-destructive visualization and analysis (XRM)</li>
<li>Q&amp;A Session with our Experts</li>
</ul>
Which Applications will be covered?
We will cover structural analysis (XRD), elemental analysis (XRF), and 3D analysis (XRM)
<ul>
<li>Different Li-battery types: NMC, NCA, LFP</li>
<li>Analysis of Battery Chemicals and Raw Materials</li>
<li>Analysis of Precursors and Cathode Active Material (CAM)</li>
<li>Analysis of Particle Size and Shape</li>
<li>Analysis of Cell Components</li>
<li>In-operando Cell Analysis</li>
<li>Cell Design and Safety Inspection</li>
<li>Black Mass Analysis during Battery Recycling</li>
<li>and more …</li>
</ul>
<blockquote>
Presenter: Dr. Michael Evans (Product Manager XRD, Bruker AXS)
</blockquote>
<blockquote>
Presenter: Dr. Adrian Fiege (Product Manager XRF, Bruker AXS)
</blockquote>
<blockquote>
Presenter: Dr. Geert Vanhoyland (Product Line Manager XRM)
</blockquote>

Bruker: From Manufacturing to Recycling: X-Ray Tech in the Battery Life Cycle

From Manufacturing to Recycling: X-Ray Tech in the Battery Life Cycle

In this live online seminar, our experts will explain what XRD, XRF and XRM can do for you!

X-Ray Tech in the Battery Life Cycle

Learn how the Agilent 4300 can easily assess coating ID, quality, authenticity and wear delivering an actionable result in less than 30 seconds.Coatings researchers and manufacturers are constantly striving to meet the ever-increasing demands on coating function, performance, and longevity.From Aerospace to Automotive, marine, and architectural coatings the versatile Agilent 4300 handheld FTIR is ideally suited to the on-site Mid IR measurement of coatings on surfaces and large objects.Knowledgeably assess factors such as identification, quality, authenticity and wear of your material or coating using the Agilent 4300 handheld FTIR.Who should attend:<ul><li>Material scientists, coating manufacturers, manufacturers who use coatings within their manufacturing process</li></ul><blockquote>Presenter: Donald Inglis (Product Specialist EMEAI for FTIR, Agilent Technologies)Donald has worked in analytical instrumentation for over 30 years starting his career as a field service engineer in chromatography and mass spectroscopy before moving into commercial sales. Becoming a product specialist in portable, handheld FTIR and Raman systems over a decade ago at Agilent Technologies.</blockquote>

Agilent Technologies: Agilent 4300 Handheld Webinar Series

Coatings Evaluation by Handheld FTIR

Learn how the Agilent 4300 can easily assess coating ID, quality, authenticity and wear delivering an actionable result in less than 30 seconds.

Agilent 4300 Handheld - Coatings Evaluation by Handheld FTIR

With the growing number and diversity of microorganisms infecting humans and animals and 2024 data showing a rise in zoonotic diseases, accurate microbiological testing is vital for detecting foodborne pathogens, spoilage organisms, and technological strains.In a food veterinary laboratory, the identification and typing of pathogens such as Salmonella, Listeria, and moulds are crucial for ensuring food safety and public health. This scientific panel focuses on advanced methodologies for detecting these microorganisms, including rapid techniques such as MALDI-TOF MS and FTIR-spectroscopy.Foodborne pathogens like Salmonella, Listeria, and moulds pose significant risks to public health, making their accurate identification and typing in food and veterinary laboratories essential. PCR, FTIR-spectroscopy and MALDI-TOF MS offer different approaches. MALDI-TOF MS identifies microorganisms based on their unique protein fingerprints, providing rapid and cost-effective results. This technique is particularly advantageous for data analysis up to species level, due to its speed, as it can deliver results within minutes once the organism is cultured.Key questions to be addressed in the panel include: Which is the recommended method for quick, broad-spectrum identification? Are MALDI-TOF MS and FTIR-spectroscopy effective tools for confirming Salmonella and Listeria? And can FTIR-spectroscopy deliver same-day identification and typing results once the organism is cultured?Furthermore, this panel will explore the latest advancements in pathogen confirmation from colony material, including new workflows for mould identification and the application of FTIR-spectroscopy for contamination root cause analysis. Attendees will also hear about new applications of FTIR-spectroscopy for faster, more accurate Salmonella and Listeria typing.&nbsp;Key learning points:<ul><li>New database content of MALDI-TOF MS</li><li>New workflow of confirmation and typing of Salmonella and Listeria by MALDI-TOF MS and FTIR-spectroscopy</li><li>New workflow for identification of moulds.</li></ul><div><blockquote>Presenter: Francis Muchaamba (Postdoc Researcher at Institute for Food Safety and Hygiene, Vetsuisse Faculty, University of Zurich )Currently Postdoc Researcher at University of Zurich. Doctor of Veterinary Medicine &amp; Biochemistry and Molecular Biology, University of Zurich, CH. Study of Veterinary Medicine at University of Zimbabwe.Presenter: Sébastien Vacher (Scientific Affairs)Nearly 20 years with &nbsp;Conidia. Research Doctorate, Microbiology at University Claude Bernard Lyon and formation sur la gestion d’entreprises, at emlyon business school.Presenter: Olaf Degen (Director Industry Microbiology)Worked for five years at Bruker and is currently Director Industry Microbiology. Microbiology Researcher at Humboldt University Berlin. Dipl.-Biologist at Freie University Berlin. MBA, Northwestern University, Evanston, IL, USA &amp; WHU, Vallendar, Germany.&nbsp;Presenter: Sarah Guerriat (Researcher at Department of Food technology, Safety and Health)Recently finished Doctor of Veterinary Medicine at University of Liège. Study of Veterinary Medicine at Université libre de Bruxelles, Belgium.</blockquote>&nbsp;</div>

New Food Magazine: Enhancing food safety labs with rapid detection of Salmonella, Listeria and moulds

Enhancing food safety labs with rapid detection of Salmonella, Listeria and moulds

Advanced methodologies for detecting microorganisms, including rapid techniques such as MALDI-TOF MS and FTIR-spectroscopy.

MALDI-TOF MS and FTIR detection of pathogens

<div><div id="container-f55ffa81be"><div><div id="container-7e6c679718"><div><div id="text-1284259899">Technologies of choice for positive material identification (PMI) in midstream and downstream operations include handheld X-ray fluorescence (XRF) and laser-induced breakdown spectroscopy (LIBS).Watch this webinar to learn about these technologies and their latest capabilities for PMI in the commissioning process or for retroactive inspection of existing assets:<ul><li>Learn the working principles of XRF and LIBS technologies.</li><li>Understand the relationship of these technologies to standards in the Oil and Gas industry such as API Recommended Practice 578 or the PHMSA Mega Rule.</li><li>Learn the latest improvements in handheld XRF and LIBS technologies along with how to choose the best option for specific PMI applications.</li><li>Hear practical examples and use cases for handheld XRF and LIBS analysis.</li></ul></div></div></div></div></div></div>

Thermo Fisher Scientific: Latest developments in PMI technologies

Latest developments in PMI technologies

Join this webinar to explore the latest capabilities of XRF and LIBS technologies for PMI.

<div>For decades, research and development (R&amp;D) has propelled the rapid pace of innovation in the semiconductor industry for developing new materials and improving manufacturing process. In many application fields, such as renewable energy (photovoltaics or hydrogen technology), aerospace and electronics, semiconductors (especially silicon) serve as fundamental and indispensable material. On the other hand, to ensure high efficiency and product quality, silicon quality control in form of identification and quantification of impurities, detection of defects or functionality test of optical devices becomes a crucial and demanding task in semiconductor industry.For semiconductor QC, among other techniques, FT-IR spectroscopy stands out as an easy and effective tool. Bruker provides a broad product portfolio to help innovating in development and process control. Phonon spectroscopy, photoluminescence, studies of band gap and electronic features using bench-top spectrometers reveal valuable information on crystal structure and quality. All-in-one Si QC system or at-line ingot analyzer dedicated for industrial environment, are highly sensitive, easy to use and optimized for saving cost in the manufacturing process.In an upcoming free-of-charge two-part webinar we will introduce you Bruker’s high sensitivity solutions for semiconductor quality control using FT-IR spectroscopy. Bench-top or at-line systems, measuring at low temperature or room temperature, Bruker can provide the suitable instrument.&nbsp;</div>

Bruker: High sensitivity Silicon QC using FT-IR Spectroscopy

High sensitivity Silicon QC using FT-IR Spectroscopy

We will introduce you Bruker’s high sensitivity solutions for semiconductor quality control using FT-IR spectroscopy.

Are you working in an analytical lab and looking for an easy and reliable FT-IR instrument for your daily work? How can you save costs in the long term, higher efficiency and reduce workload? Bruker understands you need and provides instruments with unique features that help you stand out from the crowd.FT-IR technique is an indispensable analytical tool in most chemical labs, analytical centers and quality control departments. FT-IR spectroscopy is an ease to use and non-destructive analytical method for verification, identification or quantification. To face the daily challenges arising from high sample amount, unknown materials and multiple (maybe unexperienced) users, you need a highly flexible FT-IR spectrometer with user-friendly automation and outstanding performance.Bruker cares about your need and presents you the INVENIO spectrometer platform to make your daily work easy and convenient. In the free-of-charge webinar we will focus on the difficulties in analytical labs and explain which features of INVENIO can help in such situations.

INVENIO for Analytical Centers

In the free-of-charge webinar we will focus on the difficulties in analytical labs and explain which features of INVENIO can help in such situations.

<div>Does your research involve the identification and quantification of gases?&nbsp; This webinar will focus on how Fourier-Transform Infrared (FTIR) spectroscopy is utiliztexed using different hardware and software approaches to identify the composition of complex gas mixtures with a thorough discussion of the following topics:<ul><li>Mixture analysis using library search</li><li>TGA-IR at reduced pressure&nbsp;</li><li>Spectra manipulation method for deconvoluting complex spectra (mixtures)</li></ul>Examples of applications will include the identification of plasticizers in polymers, PVC undercoating analysis, decomposition of&nbsp; PETN explosive, NHF propellant, and others.</div>

Bruker: Identification and Quantification of Gases with FT-IR

Identification and Quantification of Gases with FT-IR

This webinar explores how FT-IR spectroscopy, with various hardware and software approaches, is used to identify the composition of complex gas mixtures.

Atomic force microscopy (AFM) and its related technologies have become essential for characterizing semiconductor materials and devices, from R&amp;D to failure analysis and high-volume manufacturing.AFM's standard capability to image surface topography with nanometer-scale spatial resolution is commonly used for characterization of surface roughness, defect inspection, critical dimensions, and depth metrology with sub-nanometer precision. AFM also has the complementary ability to measure electrical, magnetic, thermal, and mechanical properties at the nanoscale. Specially equipped Bruker systems can additionally perform chemical identification at the nanoscale using patented photothermal AFM-based IR spectroscopy (AFM-IR) technology.This webinar focuses on the electrical, thermal, mechanical, and chemical AFM modes important for failure analysis:<ul><li>Electrical modes include methods for carrying out 2D carrier profiling; mapping conductivity variations, work function, and charge related characteristics; and assessing ferroelectric, piezoelectric, or dielectric properties.</li><li>The thermal mode of scanning thermal microscopy is used to measure local variations in temperature or thermal conductivity, even on active devices.</li><li>Mechanical modes are used to evaluate nanomechanical properties, such as adhesion, elastic modulus, and viscoelastic modulus.</li><li>Chemical modes can identify chemical composition of yield-killing defects and process-enabling materials, which are critical for both wafers and photomasks, especially in the EUV era.</li></ul>The presenters will introduce several modes in each of these categories and highlight physical properties characterized, spatial resolution, detection sensitivity, dynamic range, and quantification potential. They will also illustrate the capabilities and limitations of each operating mode with examples from Si-based devices and other materials, such as compound semiconductors, organic devices, and 2D materials.Presenters will also discuss practical aspects of AFM for failure analysis, such as sample preparation, probe selection and lifetime, and environmental influences.&nbsp;Join us for this webinar to hear about AFM operating modes for failure analysis, with relevant information provided for each mode, including:<ul><li>Capabilities and limitations.</li><li>Examples from Si-based devices and other materials.</li><li>Practical advice for implementation.</li></ul>By the end of the webinar, you will understand the AFM modes most valuable for failure analysis and be equipped to make informed decisions for your applications.<blockquote>Presenter: Peter De Wolf, Ph.D. (Senior Director, Research Science, Bruker)Peter De Wolf is director for AFM technology &amp; application development at Bruker Nano Surfaces, covering all applications related to Scanning Probe Microscopy (SPM). He obtained his PhD from IMEC, Belgium on the development of new SPM methods for 2D carrier profiling in semiconductors and has more than 25 years of experience on SPM. He is the author and co-author of over 30 publications related to electrical characterization using SPM. He also owns several SPM patents, and developed several new SPM modes for electrical characterization.</blockquote>

Bruker: Atomic Force Microscopy Methods for Semiconductor Failure Analysis

Atomic Force Microscopy Methods for Semiconductor Failure Analysis

Hear about AFM operating modes for failure analysis, with relevant information provided for each mode

AFM Methods for Semiconductor Failure Analysis

<header><h4>Useful Techniques for Identification and Characterization</h4></header><main><div><div><h5>Program</h5><ul><li>What are thermosets? Basic properties and formation</li><li>Thermal analysis techniques for studying thermosets</li><li>Application examples using DSC, TGA, TMA, and DMA</li><li>Which technique should be used in your analysis?</li><li>Interactive Q&amp;A session</li></ul></div></div><div><div><div>A thermoset is a polymer that undergoes a particular chemical reaction, known as curing, to form a permanent, heavily cross-linked structure. The material cannot be melted or remolded to form a new shape, even at high temperatures. Thermosets are typically rigid and insoluble, with high mechanical strength and temperature stability. Examples include epoxy resins, phenolic resins, polyesters, and polyurethanes.Due to their highly temperature-dependent physical behavior, thermal analysis is an ideal set of techniques for identifying and characterizing these materials.This webinar discusses the most important thermal properties of thermosets and describes useful thermal analysis techniques used to analyze them.Register now to secure your spot and join the live Q&amp;A!<h4>How to Characterize Thermosets</h4>Different thermal techniques can be used to determine the key properties of these materials:<ul><li>DSC: Useful for determining glass transition, melting, reaction enthalpies, curing and thermal stability.</li><li>TGA: Mainly used for composition analysis, thermal stability, decomposition, evaporation, and desorption behavior.</li><li>TMA: Typically used to study mechanical behavior such as expansion, shrinkage, softening, plus glass transition.</li><li>DMA: Best for studying viscoelastic behavior, glass transition, and frequency-dependent effects.</li></ul><h4>What is a Typical Analysis of a Thermoset?</h4>A typical and important analysis of a thermoset is the characterization of epoxy resin materials. In this case, determining the glass transition temperature (Tg) and investigating the curing reaction are highly important. This information can be used in manufacturing, for example testing the process conditions required to properly cure thermosets. It can also be used in quality control, to check the expected Tg of a known material.&nbsp;</div><div><div data-advanced-option="false" data-has-preview-image="false" data-video-id="" data-component-id="2110920040"><div style="max-width:1px;width:100%;" id="mediaContainerWrapper_2110920040"><div style="height:1px;width:1px;" data-external-url="" id="mediaContainer_2110920040" data-advanced-option="false" data-width="1" data-height="1" data-video-id="">&nbsp;</div></div></div></div></div></div></main><div><div><div data-advanced-option="false" data-has-preview-image="false" data-video-id="" data-component-id="2110920040"><blockquote><div>Presenter: Dr. Teresa Dennenwaldt</div>Dr. Teresa Dennenwaldt obtained her PhD in chemistry in 2013 and completed a postdoc at the Ecole Polytechnique Fédérale de Lausanne, Switzerland in the field of electron microscopy and spectroscopy. In 2018, she joined METTLER TOLEDO as an application specialist for Thermal Analysis. In her current position, she expertly uses, teaches, and supports DSC, TGA, TMA, and DMA instruments at the METTLER TOLEDO head office in Switzerland.</blockquote></div></div></div>

Mettler Toledo: Thermal Analysis of Thermoset Materials

Thermal Analysis of Thermoset Materials

This webinar discusses the most important thermal properties of thermosets and describes useful thermal analysis techniques used to analyze them.