The GDS900 Glow Discharge Spectrometer delivers advanced, reliable technology for routine elemental determination in electrically conductive solid materials. Designed for high-performance industrial and laboratory environments, the GDS900 combines robust hardware with intuitive Cornerstone® software to simplify operation, reporting, and data handling while reducing overall analysis time.
LECO: GDS900 Glow Discharge Atomic Emission Spectrometer
The GDS900 is optimized for bulk elemental analysis of conductive solid materials, including steel, cast iron, titanium, and other metals. When equipped with the CDP option, it also supports compositional depth profiling of treated surfaces such as galvanizing layers, plated coatings, claddings, and heat-treated materials.
Glow Discharge Spectrometry (GDS) is a direct analytical technique for determining the elemental composition of solid samples. A flat, prepared sample is mounted onto the glow discharge source, which is evacuated and then filled with argon gas. An electric field is applied between the sample, acting as the cathode, and the grounded lamp body, serving as the anode.
This setup generates a stable, self-sustained glow discharge plasma. Argon ions formed in the plasma are accelerated toward the sample surface, where they transfer kinetic energy to surface atoms through cathodic sputtering. These atoms are ejected into the plasma and become excited through collisions with energetic electrons or metastable argon atoms.
As the excited atoms return to lower energy states, they emit photons at characteristic wavelengths unique to each element. The emitted light is collected by a spectrometer whose optical system is continuously purged with argon to maintain transparency across the ultraviolet and visible range.
Photosensitive CCD detector arrays capture the full emission spectrum from 160 to 460 nm simultaneously. The resulting signals are digitized and processed to correct for dark current, normalize pixel response, extend dynamic range, and eliminate pixel artifacts. Since emitted photon intensity is proportional to elemental concentration, quantitative results are obtained through calibration with certified reference materials.
