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Fast, effective evaluation of edible bird nests using the handheld Agilent 4100 ExoScan FTIR

Applications | 2012 | Agilent TechnologiesInstrumentation
FTIR Spectroscopy
Industries
Food & Agriculture
Manufacturer
Agilent Technologies

Summary

Importance of the Topic


The edible bird nest trade commands high economic value, driven by traditional culinary uses and health claims. However, adulteration with additives such as plant materials, minerals, sugar, salt and preservatives undermines consumer confidence and poses food safety risks. Rapid and reliable authentication methods are essential to protect both industry stakeholders and end-users.

Objectives and Study Overview


This application note outlines the development of a straightforward, field-deployable approach for authenticating edible bird nests and detecting common adulterants. The study evaluates the performance of a handheld FTIR spectrometer in identifying contamination and verifying product integrity without sample destruction.

Methodology and Instrumentation


  • Instrument: Agilent 4100 ExoScan FTIR handheld mid-IR system equipped with a diffuse reflectance interface for non-destructive sampling.
  • Power and portability: Rechargeable lithium-ion batteries enabling four hours of continuous operation; optional docking for lab-bench performance equivalence.
  • Software: Agilent MicroLab Mobile FTIR software implementing a quantitative pass/fail method for real-time adulterant identification.

Key Results and Discussion


  • Calcium carbonate contamination: Detected by characteristic diffuse-reflectance bands at 1410 cm−1 and 873 cm−1, distinguishing cave-derived mineral residues.
  • Salt adulteration: Sodium chloride lowers sample absorption, inverting negative bands to positive on an absorbance scale.
  • Sucrose addition: Identified by strong bands at 1050, 980 and 905 cm−1, confirmed by comparison with reference ATR spectra.
  • Monosodium glutamate (MSG): Revealed through an amide I doublet overlapping protein bands, indicating glutamate presence.

Benefits and Practical Applications


The handheld FTIR approach offers rapid, on-site screening for unskilled operators using a simple select-point-press workflow. Multiple areas of each nest can be tested non-destructively, enabling immediate rejection of adulterated products and enhancing supply-chain integrity.

Future Trends and Opportunities


Advances may include further miniaturization, integration of machine learning for automated spectral interpretation, expansion of adulterant spectral libraries, and broader deployment in food safety inspections and quality control.

Conclusion


Handheld FTIR spectroscopy provides an efficient, sensitive, and non-destructive solution for authenticating edible bird nests. Its ease of use, portability and robust quantitative methods support rapid decision-making and help safeguard product authenticity and consumer health.

References


  1. Li, X., Xi, X. & Che, W. (2003) Analysis and assessment of quality in import-export bird nest. Guangzhou Food Science and Technology, 19:72–89.

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