<h3><strong>Lunch &amp; learn tips &amp; tricks series 2026 – part 1</strong></h3><p><strong>In modern analytical laboratories, efficiency, consistency, and data confidence are essential. Whether you are operating an ICP-OES or ICP-MS system, the way you use your software can significantly influence productivity and analytical performance. In the first session of our Lunch &amp; Learn Tips &amp; Tricks Series, we focused on one of the most common themes raised by users: how to navigate </strong><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/products/1489"><strong>Qtegra </strong></a><strong>software more effectively and optimize everyday workflows.</strong></p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/Thermo_Fisher_Scientific_Mastering_Qtegra_Software_Practical_Strategies_to_Improve_Your_Daily_Lab_Workflow_3d35454782.jpg" alt="Thermo Fisher Scientific: Mastering Qtegra Software: Practical Strategies to Improve Your Daily Lab Workflow" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_Thermo_Fisher_Scientific_Mastering_Qtegra_Software_Practical_Strategies_to_Improve_Your_Daily_Lab_Workflow_3d35454782.jpg 245w," sizes="100vw" width="1024" height="512"></p><p><strong>This session explored three key areas in detail: </strong>understanding the structure of Qtegra and the Configurator, using the Dashboard as your operational control center, and building smarter, more efficient LabBooks. Below is a structured recap of the key insights shared during Part 1.</p><h3><strong>Understanding the structure of Qtegra</strong></h3><p>One of the most valuable features of Qtegra software is its consistency across multiple instrument platforms. Whether you are working with the <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/products?category=227&amp;instrumentationItems=84&amp;manufacturerItems=3&amp;search=icap+pro"><strong>iCAP PRO ICP-OES</strong></a>, the <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/products?category=232&amp;instrumentationItems=83&amp;manufacturerItems=3"><strong>iCAP MX ICP-MS</strong></a>, the iCAP 7000 OES, or Qnova ICP-MS systems, the interface and workflow logic remain familiar. This consistency reduces the learning curve when transitioning between instruments and supports standardised training across laboratories.</p><p><strong>Qtegra consists of two primary components:</strong> the Qtegra application itself and the Configurator.</p><ul><li><strong>The Qtegra application</strong> is where you directly interact with your instrument. It is used to create LabBooks, control the instrument, execute analyses, and review results.</li><li><strong>The Configurator</strong>, in contrast, defines how your system behaves at a deeper level. It controls system-level settings that underpin daily operation. Within the Configurator, users can manage features such as Fast Uptake setup, drain sensor configuration, wavelength libraries for ICP-OES systems, the Reaction Database for ICP-MS systems, and user access permissions.</li></ul><p>Understanding the distinction between these two components helps users troubleshoot more effectively and ensures that system configuration aligns with laboratory requirements.</p><h3><strong>Using the dashboard as your central hub</strong></h3><p>When Qtegra is opened, the first screen presented is the Dashboard. The Dashboard functions as the central hub for instrument monitoring and control. From this location, users can view instrument status, monitor live operating parameters, access tuning tools, review performance checks, and identify error or interlock notifications.</p><ul><li><strong>For ICP-OES users</strong>, the Dashboard provides access to tune sets, source settings, AutoPeak alignment, autotuning functions, and live views such as Plasma TV. These tools allow users to confirm that the plasma and optical system are performing as expected before analysis begins.</li><li><strong>For ICP-MS users</strong>, the Instrument tab within the Dashboard provides access to autotune routines, performance report summaries, gas flow settings, nebuliser adjustments, operating mode selection such as Standard, KED, or CCT modes, IntelliLens control, and real-time data streams.</li></ul><p>The Dashboard should be used as a structured checkpoint before running any analysis. Confirming that all parameters are within acceptable ranges reduces the likelihood of interruptions and supports consistent performance throughout the run.</p><h3><strong>The get ready workflow: structured instrument preparation</strong></h3><ul><li><strong>The Get Ready function</strong>, which is launched directly from the Dashboard, provides a guided preparation workflow. This feature is designed to ensure that the instrument is fully configured and operating correctly for the selected method before analysis begins.</li><li><strong>Within Get Ready</strong>, users can access scheduling tools that automate warmups, standby routines, shutdowns, and maintenance checks. These tools are particularly beneficial for laboratories operating multiple shifts or managing variable workloads.</li></ul><p>For<strong> ICP-MS systems</strong>, the Get Ready workflow includes automated performance checks, autotune routines, and controlled warm-up conditions. These routines verify that the instrument is operating within its expected performance range.</p><p>By following the structured steps within Get Ready, laboratories can reduce the risk of missed preparation tasks and maintain day-to-day analytical consistency.</p><h3><strong>Building smarter LabBooks</strong></h3><p>The LabBook forms the foundation of every analytical sequence in Qtegra. A carefully constructed LabBook improves efficiency, reduces setup errors, and simplifies data review.</p><p>Users can create a LabBook from scratch or begin with a template. Templates are particularly useful for laboratories that integrate with LIMS systems or import sample lists via CSV files, as they promote standardisation and consistency.</p><h4><strong>Defining analytes</strong></h4><ul><li><strong>For ICP-OES methods</strong>, users must select appropriate wavelengths and evaluate potential spectral interferences.&nbsp;</li><li><strong>For ICP-MS methods</strong>, users select the required masses, consider isobaric and polyatomic interferences, and use the Reaction Database to support reaction mode selection.</li></ul><p>Careful analyte selection at this stage helps prevent complications later in the analytical workflow.</p><h4><strong>Configuring acquisition parameters</strong></h4><p>Acquisition parameters define how the instrument collects data.</p><ul><li><strong>For ICP-OES systems</strong>, this includes selecting viewing modes, choosing wavelength ranges such as iFR or eUV, and defining integration times.</li><li><strong>For ICP-MS systems</strong>, this includes selecting operating modes such as Standard, KED, or CCT, configuring Reaction Finder options, enabling Intelligent Matrix Handling, and defining digital trigger settings.</li></ul><p>Thoughtful parameter configuration ensures that data quality objectives are met without unnecessary reanalysis.</p><h4><strong>Using intelligent uptake and rinse</strong></h4><p>The Intelligent Uptake and Rinse feature detects when the sample or rinse solution reaches the nebuliser. This ensures consistent timing across samples and improves overall throughput. In high-throughput environments, this feature contributes to both efficiency and reproducibility.</p><h4><strong>Calibration and quantification strategy</strong></h4><p>Calibration design is central to reliable quantification. Qtegra allows users to manage global standards, configure dilution tools, select calibration fit types, assign internal standards, and establish quality control samples.</p><p>For ICP-OES systems, users can define standard ranges and switch points. For SemiQuant workflows, Relative Sensitivity Factors can be applied.</p><p>Establishing these parameters during LabBook creation ensures that data validation is straightforward once analysis is complete.</p><h4><strong>Autosampler and sample list setup</strong></h4><p>For laboratories using the <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/products/1715"><strong>iSC-65 autosampler</strong></a>, features such as StepAhead, custom rack definitions, colour-coded sample views, and visual integrity checks support efficient sequence management.</p><p>When constructing the sample list, users should clearly define sample types, establish a logical sequence order, and configure column layouts appropriately. Setting flags and limits during initial setup simplifies the data review process and supports quality assurance.</p><h3><strong>Why workflow optimisation matters</strong></h3><p>Optimising Qtegra usage does not require learning new software features. Instead, it involves using existing tools more strategically. By treating the Dashboard as a pre-run checkpoint, using Get Ready consistently, and constructing LabBooks with long-term efficiency in mind, laboratories can reduce downtime, improve reproducibility, and strengthen confidence in analytical results.</p><h3><strong>Looking ahead to part 2</strong></h3><blockquote><p><strong>In Part 2 of the Qtegra Tips &amp; Tricks series</strong>, we will focus on post-analysis best practices. Topics will include interpreting signal intensities, reviewing calibration performance, evaluating recoveries and readbacks, applying flags effectively, exporting data, and implementing practical workflow improvements discussed in Part 1.</p></blockquote><p>By building a structured approach to both preparation and data review, laboratories can transform routine analysis into a streamlined, reliable, and repeatable process.</p><p>We look forward to continuing the discussion in <strong>Part 2</strong>.</p><h5><strong>Acknowledgement</strong></h5><p>I would like to thank <strong>Matthew Gregory </strong>Field Applications Scientist, North EMEA, Trace Elemental Analysis and <strong>David Fishwick </strong>Field Applications Scientist, North EMEA, Trace Elemental Analysis for the support on this blog and the webinars</p><h4><strong>Sign up for our webinars live and on demand.</strong></h4><p><strong>English</strong></p><ul><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/5795"><strong>Lunch and Learn Tips and Tricks Series: Qtegra Part 1</strong></a></li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/5976"><strong>Lunch and Learn Tips and Tricks Series: Qtegra Part 2</strong></a></li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/5977"><strong>Lunch and Learn Tips and Tricks Series: Trace Elemental Analysis (ICP-OES &amp; ICP-MS)</strong></a></li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/webinar/5978"><strong>Trace Elemental Analysis: Ask the Expert</strong></a></li></ul><p><strong>Deutsch</strong></p><ul><li><strong>19. März 2026</strong> <a target="_blank" rel="noopener noreferrer" href="https://event.on24.com/wcc/r/5179134/393E071E3B501943730958BA6203F477">Interne Standards in der ICP-OES: Ein Praxisguide für zuverlässige Qualitätssicherung im Labor</a></li><li><strong>18. Juni 2026</strong> <a target="_blank" rel="noopener noreferrer" href="https://event.on24.com/wcc/r/5179292/AE4C576B6A54D1AC182F7F77573D380F">Fehler reduzieren, Durchsatz steigern: Autoverdünnung mit PrepFast am ICP-MS</a></li><li><strong>17. September 2026</strong> <a target="_blank" rel="noopener noreferrer" href="https://event.on24.com/wcc/r/5179423/B5019C560431BADCA2A76E54E4EFE56F">ICP-OES smarter nutzen: Probendurchsatz erhöhen, Ressourcen sparen</a></li><li><strong>17. Dezember 2026</strong> <a target="_blank" rel="noopener noreferrer" href="https://event.on24.com/wcc/r/5179530/94EEDD1F56138F5EEE2AF24E29E6C12A">Qtegra ISDS Software Unlocked – Live im Expertengespräch</a></li></ul><p><strong>Visit us on&nbsp;</strong><a target="_blank" rel="noopener noreferrer" href="https://www.linkedin.com/showcase/72003132/admin/dashboard/"><strong><u>LinkedIn:</u></strong></a><strong>&nbsp;</strong>#Qtegra, #ICPMS, #ICPOES, #TraceElementalAnalysis</p><blockquote><h5><strong>Petra Gerhards</strong></h5><p>Petra Gerhards, Dipl-Ing, is Regional Marketing Manager of GC and GC-MS for EMEA at Thermo Fisher Scientific. She has more than 29 years of experience in the fields of GC-MS, SPE and LC-MS. Since joining the regional team she has contributed to workflow solutions combining vials and closures with SPE solutions, GC-MS and LC-MS. She works with KOL's on data for regional specific marketing campaigns, organizes in-house seminars and works on customer specific solutions. Her main expertise is in the field of doping and drugs-of-abuse analysis.</p></blockquote>

Mastering Qtegra Software: Practical Strategies to Improve Your Daily Lab Workflow

<p><strong>Since the beginning of this year, a project to develop a light-based electron microscope, LightEM, has been underway at CEITEC Brno University of Technology (BUT). The principal investigator is Andrea Konečná from CEITEC BUT and the Faculty of Mechanical Engineering BUT, who has secured support for the project through the prestigious ERC CZ program. Over the next five years, her research team aims to develop and test a light-based electron microscope. This technology would allow scientists to adaptively modulate the electron beam during experiments or observe processes over time – capabilities that are not possible with conventional electron microscopes.</strong></p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/CEITEC_VUT_Vaclav_Konicek_Mikroskop_budoucnosti_Spojeni_svetla_a_elektronu_ziskalo_prestizni_grant_4_2062655721.jpeg" alt="CEITEC/Václav Koníček: Microscope of the Future: Combining Light and Electrons Wins Prestigious Grant: Andrea Konečná's group" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_CEITEC_VUT_Vaclav_Konicek_Mikroskop_budoucnosti_Spojeni_svetla_a_elektronu_ziskalo_prestizni_grant_4_2062655721.jpeg 235w," sizes="100vw" width="1600" height="1067"></p><p>Over the coming five years, Andrea's team will work on improving existing electron microscopes. Her project,<strong> Light-Based Electron Microscope </strong>(LightEM), focuses on the interaction between electrons and light and could help overcome some of the limitations of classical electron microscopy. <i>“We are trying to improve the electron beam. What we want to do is, figuratively speaking, shoot an intense laser beam into the microscope and influence electrons using light. Simply put, we aim to create adjustable ‘glasses’ for the electron microscope using light and change how optics is traditionally done in electron microscopy,”</i> explained Andrea.</p><p>According to her, this approach should bring <strong>higher resolution, new imaging techniques, and the ability to study dynamic processes</strong>. <i>“With light, the resolution should be even better. Moreover, we could image sensitive samples, which is usually problematic. We could also observe processes over time </i>–&nbsp;<i>stimulate a sample with light, for example by heating it, and then dynamically monitor what is happening,”</i> she added.</p><h3><strong>The microscope will offer better resolution and new imaging techniques</strong></h3><p>Andrea points out that standard electron microscopes use magnetic lenses to image and focus electrons onto a sample, but these lenses have imperfections that limit resolution. The best electron microscopes in the world therefore use many lenses – similar to professional camera lenses – to compensate for these defects and achieve atomic resolution. A light-based electron microscope could change this.</p><p><i>“We would like to demonstrate that such complex lens systems </i>–&nbsp;<i>whose production, alignment, and operation are very expensive and demanding </i>–&nbsp;<i>could be replaced by a specially modulated laser beam. Compared to conventional lenses, a laser beam can be used not only for magnification, reduction, or aberration correction, but also offers great flexibility and the possibility to create new ‘exotic’ types of electron beams. Electrons don’t have to be focused only into a point; we can create a beam shaped like a ‘donut.’ In addition, the beams could be modulated quickly and adaptively,</i>” said Andrea.</p><p>According to her, such a modified microscope could be used in many fields. <i>“Thanks to the possibility of light-based modulation of the electron beam during experiments, we could more efficiently image sensitive samples, which is crucial for biology. Or we could detect defects in materials and semiconductor components more quickly,”</i> she added.</p><p>This is highly unique research with no equivalent in scope, either in the Czech Republic or abroad. According to Andrea, only a few studies on the topic have been published so far. <i>“At the time I was writing the grant, only a few theoretical and experimental papers had demonstrated the basic concept </i>–&nbsp;<i>that electrons can be focused or otherwise modulated using a laser beam. But they did not go as far as we would like, namely to create a prototype microscope where part of the standard electron optics is replaced by a laser beam</i>,” she said.</p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/CEITEC_VUT_Vaclav_Konicek_Mikroskop_budoucnosti_Spojeni_svetla_a_elektronu_ziskalo_prestizni_grant_3_1ec4c49bf5.jpeg" alt="CEITEC/Václav Koníček: Microscope of the Future: Combining Light and Electrons Wins Prestigious Grant: Andrea Konečná's research" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_CEITEC_VUT_Vaclav_Konicek_Mikroskop_budoucnosti_Spojeni_svetla_a_elektronu_ziskalo_prestizni_grant_3_1ec4c49bf5.jpeg 235w," sizes="100vw" width="1600" height="1067"></p><h3><strong>Unique research supported by the Ministry of Education</strong></h3><p>The project’s strong potential is confirmed by the fact that Andrea Konečná received an <strong>ERC CZ grant from the Czech Ministry of Education, Youth and Sports</strong>. The program aims to support researchers who applied for a<strong> European ERC grant</strong>, succeeded in evaluation, but were not funded due to limited resources.</p><p><i>“There is enormous competition within the European ERC program. I submitted this project twice and both times advanced to the second round, where I presented it and discussed it with the panel. Each time I received an A rating, but unfortunately without funding. The Ministry looks at these European evaluations and ultimately supported my project. To be honest, it is mainly about prestige, because otherwise the conditions are the same. The project still runs for five years, and the Ministry supported it in full, so we receive the same funding we would have received from the European Union,”</i> Andrea noted.</p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/CEITEC_VUT_Vaclav_Konicek_Mikroskop_budoucnosti_Spojeni_svetla_a_elektronu_ziskalo_prestizni_grant_2_3114b2e414.jpeg" alt="CEITEC/Václav Koníček: Microscope of the Future: Combining Light and Electrons Wins Prestigious Grant: Andrea Konečná's research" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_CEITEC_VUT_Vaclav_Konicek_Mikroskop_budoucnosti_Spojeni_svetla_a_elektronu_ziskalo_prestizni_grant_2_3114b2e414.jpeg 235w," sizes="100vw" width="1600" height="1067"></p><h3><strong>Two prestigious grants – and motherhood alongside</strong></h3><p>A few years ago, Andrea Konečná also received the <strong>prestigious JUNIOR STAR grant</strong> from the <strong>Czech Science Foundation</strong>, which supports outstanding early-career researchers. She is currently the principal investigator of two major projects, while also balancing motherhood since last year.</p><p><i>“Maybe it’s still too early to evaluate, because my daughter is still small and I was on maternity leave for some time. But honestly, it is demanding. At the same time, the flexibility of our work makes it easier than in other professions. Moreover, the JUNIOR STAR project is already in its fourth year, and several excellent PhD and master’s students have joined during that time, so many smaller projects were able to continue even during my maternity leave. I’m also happy that several of these colleagues will now join the ERC CZ project,”</i> she concluded.</p><p><img src="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/CEITEC_VUT_Vaclav_Konicek_Mikroskop_budoucnosti_Spojeni_svetla_a_elektronu_ziskalo_prestizni_grant_1_8369f441d5.jpeg" alt="CEITEC/Václav Koníček: Microscope of the Future: Combining Light and Electrons Wins Prestigious Grant: Andrea Konečná" srcset="https://storage.googleapis.com/labrulez-bucket-strapi-h3hsga3/thumbnail_CEITEC_VUT_Vaclav_Konicek_Mikroskop_budoucnosti_Spojeni_svetla_a_elektronu_ziskalo_prestizni_grant_1_8369f441d5.jpeg 235w," sizes="100vw" width="1600" height="1067"></p><h3><strong>A major success for CEITEC Brno University of Technology</strong></h3><p><i>“I greatly appreciate the success of Andrea Konečná, who managed to succeed in a highly competitive environment. It is the result of long-term high-quality scientific work and significant personal dedication. At the same time, I am pleased that at BUT, we are systematically creating conditions to support excellent research. One of the key tools is the <strong>Research Excellence Support Fund</strong>, through which we <strong>motivate and support researchers in preparing applications for prestigious grants</strong> such as <strong>ERC, EXPRO, JUNIOR STAR, or MSCA</strong>. These are precisely the types of projects that push the boundaries of knowledge and strengthen the international standing of our university,”</i> said <strong>Martin Weiter</strong>, Vice-Rector of BUT for Research and Knowledge Transfer.</p>

Microscope of the Future: Combining Light and Electrons Wins Prestigious Grant

<p><strong>Our Library never stops expanding. What are the most recent contributions to LabRulezICPMS Library in the week of 30th March 2026? Check out new documents from the field of spectroscopy/spectrometry and related techniques!</strong></p><blockquote><p><span style="font-size:20px;">👉 </span><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/library"><span style="font-size:20px;"><strong>SEARCH THE LARGEST REPOSITORY OF DOCUMENTS ABOUT SPECTROSCOPY/SPECTROMETRY RELATED TECHNIQUES</strong></span></a></p></blockquote><blockquote><p><strong>👉 Need info about different analytical techniques?</strong> Peek into <a target="_blank" rel="noopener noreferrer" href="https://lcms.labrulez.com/library"><strong>LabRulezLCMS</strong></a> or <a target="_blank" rel="noopener noreferrer" href="https://gcms.labrulez.com/library"><strong>LabRulezGCMS</strong></a> libraries.</p></blockquote><p>This week we bring you application notes by <strong>Metrohm,</strong> <strong>Shimadzu, Thermo Fisher Scientific </strong>and <strong>Waters Corporation!</strong></p><h3><strong>1. Metrohm: Quantification of methanol in contaminated spirits</strong></h3><p><strong>Protecting consumers from contaminated beverages</strong></p><ul><li>Application note</li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/labrulez-bucket-strapi-h3hsga3/an_rs_056_download_3b37cb883a.pdf"><strong>Full PDF for download</strong></a></li></ul><p>An alarming global trend highlights the serious harm that can result from ingesting illegal, improperly distilled alcohol. Home-distilled spirits prepared using industrial solvents (i.e., wood alcohol) and presented as legitimate alcoholic beverages often contain methanol. Methanol causes blindness and can lead to death when ingested. This has led to fatal consequences around the world [1–3].&nbsp;</p><p>The breaking point for the Czech Republic came in September 2012. The sale of hard liquor was temporarily banned after 20 people died from the consumption of spirits with dangerous levels of methanol [2]. After an exhaustive study using various screening tools, the Czech Republic adopted Raman spectroscopy as the method of choice for identifying and quantifying methanol in contaminated spirits. This Application Note demonstrates how Raman spectroscopy can be employed as an efficient and rapid screening method for samples of rum contaminated with methanol.</p><h4><strong>EXPERIMENT&nbsp;</strong></h4><p>This example study measures commercially available coconut rum that is spiked with methanol in concentrations between 0.33% and 5.36%. The <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/library?mainauthorItems=220&amp;search=iRaman"><strong>iRaman NxG 785H</strong></a> with a fiber-optic probe is used to collect Raman spectra of the mixtures (Figure 3). Table 1 lists the relevant equipment and instrument settings used for this application study. The peak at around 1000 cm-1 (highlighted by the inlay of Figure 3) visibly increases with increasing concentration of methanol, becoming significant at approximately 1%.</p><h4><strong>CONCLUSION</strong></h4><p>These results validate that Raman spectroscopy can be used for rapid, quantitative screening of dangerous adulterants in alcoholic beverages. This technique can be expanded to investigate adulteration in other media such as food, petroleum, and pharmaceutical drugs [4].</p><h3><strong>2. Shimadzu: Evaluation of Organic Impurities in Lithium Carbonate by TOC Analysis</strong></h3><ul><li>Application note</li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/labrulez-bucket-strapi-h3hsga3/an_01_01098_en_ec9b3e73fc.pdf"><strong>Full PDF for download</strong></a></li></ul><h4><strong>User Benefits</strong></h4><ul><li>TOC analysis enables effective control of organic impurities in lithium carbonate.</li><li>Using the combustion tube kit for high-salt samples can extend the lifespan of the combustion tube and catalyst, reducing maintenance frequency.</li><li>With the <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/library?mainauthorItems=1&amp;search=ASI-L+autosampler"><strong>ASI-L autosampler</strong></a>, multiple samples can be measured automatically, improving throughput and efficiency</li></ul><p>Lithium carbonate (Li2CO3) is an important material used in a wide range of applications in the lithium-ion battery industry. For example, it is used as a lithium source for cathode active material synthesis and electrolyte salt production, as a raw material for oxide-based solid electrolytes, and as a form of lithium commonly recovered in recycling processes.&nbsp;</p><p>Because impurities in lithium carbonate can affect downstream processes and final products, appropriate control is essential. In particular, organic impurities require especially careful attention because they may originate from so many sources, such as solvents and processing aids used during purification, residual organics from manufacturing steps, or contamination introduced during handling and storage.&nbsp;</p><p>Total organic carbon (TOC) analysis offers an effective way to manage such organic impurities in raw materials. This article presents an example of using a <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/library?mainauthorItems=1&amp;search=TOC-L"><strong>Shimadzu TOC-L</strong></a> total organic carbon analyzer (Fig. 1) to evaluate the TOC content of lithium carbonate.</p><h4><strong>TOC Analysis&nbsp;</strong></h4><h5><strong>TOC Analysis Methods&nbsp;</strong></h5><p>Two commonly used methods are available for TOC analysis:&nbsp;</p><p><strong>(1) TC - IC method: </strong>Total carbon (TC) and inorganic carbon (IC) are measured separately, and then TOC is calculated as the difference (TOC = TC – IC).</p><p><strong>(2) NPOC method: </strong>TOC is measured as non-purgeable organic carbon (NPOC). After acidifying the sample to pH &lt; 3, IC is subsequently removed by sparging and the remaining carbon is measured as TC, which is regarded as TOC. The acidification and sparging steps are performed automatically by the instrument.&nbsp;</p><p>For lithium carbonate solutions, the amount of carbonatederived IC is typically very high. As a result, the TC–IC method tends to yield calculated TOC values with a larger relative error. Therefore, the NPOC method isrecommended.</p><p>&nbsp;In lithium carbonate solutions prepared as described above, IC is expected to be present mainly as bicarbonate (HCO<sub>3</sub> <sup>–</sup>) and carbonic acid (H<sub>2</sub>CO<sub>3</sub>). If IC is not fully removed during NPOC pretreatment, the TOC result may be overestimated. Therefore, thorough IC removal is critical for samples with high IC content. For actual samples, sparging parameters, such as sparge gas flow rate and sparge time settings, can be adjusted.&nbsp;</p><h5><strong>Combustion Tube for High-Salt Samples&nbsp;</strong></h5><p>The prepared lithium carbonate solution contains a large amount of salts. When a large number of salt-containing samples are analyzed, salts may accumulate inside the combustion tube, which can lead to catalyst clogging, reduced sensitivity, and poorer repeatability.</p><p>For this analysis, the optional combustion tube for high-salt samples was used, shown in Fig. 2. The high-salt combustion tube has a larger diameter than the standard combustion tube and contains larger catalyst particles to help mitigate saltrelated clogging. Thus, the frequency of combustion tube replacement can be significantly reduced.</p><h4><strong>Conclusion&nbsp;</strong></h4><p>In this article, TOC analysis was performed for a 10 g/L lithium carbonate solution using a Shimadzu TOC-L total organic carbon analyzer. By measuring TOC in the prepared solution, the TOC content in the lithium carbonate solid was calculated. The results showed good recovery rates in the spike-recovery test and consistent performance was also confirmed during long-term continuous analysis. These findings demonstrate that the TOC-L is a reliable solution for measuring TOC in lithium carbonate and for effective management of organic impurities.&nbsp;</p><p>When applying the NPOC method to lithium salt-containing solutions, careful selection of the acid is essential because salts formed during acidification can affect both data quality and instrument condition. For this example, sulfuric acid is recommended.</p><p>In addition, using the optional combustion tube kit for high-salt samples can extend the lifespan of the combustion tube and catalyst, thereby reducing maintenance frequency. This option is especially helpful for samples with high salt concentrations.&nbsp;</p><p>In addition to lithium carbonate, the TOC-L can also be applied to TOC analysis of lithium hydroxide solutions, determination of water-extractable TOC in recycled black mass, and analytical needs in lithium refining processes based on direct lithium extraction (DLE). With its broad applicability across various upstream materials, recycling streams, and refining processes, the TOC-L supports both quality control and process optimization operations throughout the lithium-ion battery value chain.</p><h3><strong>3. Thermo Fisher Scientific: Evaluating Silicon using Raman Microscopy</strong></h3><ul><li>Application note</li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/labrulez-bucket-strapi-h3hsga3/vib_silicon_analysis_with_raman_microscope_app_note_mcs_an1232_en_11_2024_1887815_web_50639c9148.pdf"><strong>Full PDF for download</strong></a></li></ul><p>Raman spectroscopy is a form of vibrational spectroscopy that probes chemical bonds and molecular structure and is sensitive to small changes in chemical and structural environments. The Raman spectrum of a material is a molecular “fingerprint” that can be used for identification of unknown materials and for characterizing and qualifying expected materials. Since intermolecular effects and lattice vibrations are also detected, it can be used to evaluate crystallinity. Mechanical phenomena such as strain can also be detected from peak shifts in Raman spectra. Raman imaging allows visualization of the distribution of components or changes in physical state across the sample.</p><h4><strong>Silicon in aluminum&nbsp;</strong></h4><p>Silicon is used in alloys with aluminum to increase the strength of lightweight aluminum-based parts. Addition of silicon to aluminum also alters the viscosity of melted aluminum, improving the castability. These alloys typically contain 3% to 25% silicon. While silicon and aluminum can form a eutectic mixture, it is common to have finely dispersed silicon particles throughout the material.¹ The size and distribution of silicon particles can affect the strength of the aluminum.&nbsp;</p><p>One common example of an aluminum product, aluminum foil, is made up of almost pure aluminum (approximately 98.5%) but it does contain small amounts of silicon and iron.² Raman imaging of a piece of aluminum foil reveals small particles of silicon (Figure 1). A <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/products/2237"><strong>Thermo Scientific™ DXR3xi Raman Imaging Microscope </strong></a>was used with a 532 nm laser and a 100X&nbsp;metallurgical objective to collect the Raman imaging data. An area of 408 μm x 208 μm was imaged using an image pixel size of 1 μm. The Raman image, based on the 520 cm-1 peak of silicon, shows the spatial distribution of the particles and image analysis provides size and shape information. In this case, 81&nbsp;silicon particles were identified with a size (area) range of 6-151 μm². This analytical approach may be extrapolated to other types of Si/Al alloy parts.</p><h4><strong>Conclusion&nbsp;</strong></h4><p>The importance of silicon as a technologically significant material cannot be overstated. It has properties that make it useful in numerous different types of products. Raman micro-spectroscopy has proven itself an important tool for the assessment of molecular structure and physical states of silicon. Raman images provide a way to observe the spatial distribution of silicon and silicon-containing components, structural variations such as crystallinity, and physical effects such as strain. This note showed a few representative examples to illustrate some of the advantages offered by Raman microscopic analysis of silicon. The coverage is not intended to be comprehensive as there are numerous other areas where the Raman analysis of silicon is currently employed and other opportunities where it could be used. The Thermo Scientific DXR3 Raman Microscope and the Thermo Scientific DXR3xi Raman Imaging Microscope have both been shown to be excellent choices for the Raman analysis of silicon samples.</p><h3><strong>4. Waters Corporation: High-Throughput Detection of Degraded Polysorbate in Biological Formulations with FMM</strong></h3><ul><li>Application note</li><li><a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/labrulez-bucket-strapi-h3hsga3/720009114_en_99c7483d1a.pdf"><strong>Full PDF for download</strong></a></li></ul><p>The FDA requires that all biologic formulations be free of visible particles and has defined allowable levels of subvisible particles (SVPs) larger than 10 µm to ensure the potency, efficiency, and safety of these drug.<sup>1</sup> While most protein drug particle analysis focuses on particles formed due to formulation instability, SVPs formed through the degradation of formulation excipients must also be considered.&nbsp;</p><p>Polysorbates 20 (PS20) and 80 (PS80), best known as Tween-20 and -80, are excipients used in &gt;70% of marketed parenteral biological drugs to improve product stability and shelf life.<sup>2</sup> However, when these formulations are stored for long periods of time (&gt;6 months) at low temperatures (4 °C), visible and subvisible particles are formed due to the enzymatic hydrolysis of the polysorbates by host cell proteins (HCPs) such as esterases and lipases.<sup>3,4</sup> PS20 in particular has been found to be extremely prone to degrading into fatty acid particles.<sup>5</sup> Lauric, myristic and palmitic acids are the most common fatty acid degradation products, and there is a direct correlation between low fatty acid solubility and particle formation in common formulation buffers.<sup>3–7</sup> However, high-throughput, sensitive, and specific analysis of polysorbate particles has been difficult due to their complex chemistry and their low concentrations (&lt;&lt;0.5%) in high protein concentration (&gt;100–200 mg/mL) formulation environments, making it a perennial needle in a haystack problem.</p><p>In this application note, we introduce the Aura™ polysorbate degradation assay, a specific and quantitative assay that detects free fatty acid particles (FFAs) formed during polysorbate degradation on Aura PTx System. The assay analyzes 96 samples using anywhere from 5 µL–10 mL of sample in a few hours. <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/products/2190"><strong>Aura™ Systems</strong></a> use backgrounded membrane imaging (BMI) and fluorescence membrane microscopy (FMM) to count, size and ID particles from 1 µm to 5 mm. Fluorescent labels utilized by FMM are selected based on thier ability to interact with particles of a certain nature, allowing for the generation of key information related to identity of the particles.</p><h4><strong>Results and Discussion&nbsp;</strong></h4><h5><strong>Morphological Appearance of Different Fatty Acid Particles&nbsp;</strong></h5><p>Aura systems image every particle, enables subvisible particle size distributions analysis, and makes morphological differentiation possible using built-in image analysis filters. When we analyze different free fatty acid solutions with Aura PTx System, we find that each forms particles with different morphological characteristics. Lauric acid particles are large and irregular clusters, myristic acid particles are small and oval shaped, and palmitic acid particles form fibril-like particles and small circular clusters (Figure 2a-c). These unique morphological characteristics suggest the presence of free fatty acid particles that can then be confirmed with FMM using labeled fluorescence.</p><h4><strong>Conclusion&nbsp;</strong></h4><p>Aura PTx System and <a target="_blank" rel="noopener noreferrer" href="https://icpms.labrulez.com/products/2190"><strong>Aura+ System</strong></a> can easily detect the major degradation components of PS20 in proteincontaining samples at any stage of the drug manufacturing process. The method only requires 5 µL of sample, is specific and sensitive, and can analyze 96 samples in just a few hours, far outperforming other techniques. Aura PTx System and Aura+ System can also identify and differentiate the key degraded particulates from polysorbate formulation by their distinguishable shape, appearance, and specific labeling with BODIPY FL C16. The Aura polysorbate assay can detect FFAs at concentrations relative to lauric acid above 9.38 µM (&gt;2183 counts/mL) and quantitate above 18.75 µM (&gt;2976 counts/mL).</p>

News from LabRulezICPMS Library - Week 14, 2026

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Since its establishment in 2011, CEITEC has quickly developed into a cutting-edge infrastructure for research which performs highly alongside the best institutes in Europe. Among the main priorities of CEITEC are the promotion of a motivating and dynamic international scientific environment, the provision of state-of-the-art research infrastructure, and the policy of open communication and equal opportunities.

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A unique company dedicated to serving science helping our customers drive productivity and accelerate results. Through our premier brands – Thermo Scientific, Applied Biosystems, Invitrogen, Fisher Scientific and Unity Lab Services.

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<p><strong>The second Pharma Virtual Symposium offers you innovative solutions that address the challenges you face day to day in your lab. Visit the virtual booths to explore workflow &amp; compliance solutions. Explore “Tomorrow’s technologies for today” to improve efficiency, productivity &amp; reduce the compliance risks.</strong></p>
<h5><strong>The symposium will be following these two tracks:</strong></h5>
<ul>
<li>Day 1- Pharmaceutical Workflow For Development To QC</li>
<li>Day 2 - Pharmaceutical Workflow for Impurities</li>
</ul>
<p>Come and explore the world of pharmaceutical solutions which have been developed keeping your daily problems in mind.</p>
<h5><strong>What’s inside the Pharma Virtual Symposium?</strong></h5>
<ul>
<li>Live Webinars from Agilent Experts</li>
<li>Virtual Exhibition with detailed Booths and Application Notes</li>
<li>Live Chat with Experts from your local region</li>
<li>Comprehensive Resource Centre with relevant collaterals for the Pharma Market</li>
<li>Demo Lab with videos about how our Instruments work</li>
</ul>
<p>Join this Symposium and feel free to get involved, ask questions, make suggestions and be a part of the community.</p>
<h3><strong>Day 1 -Pharmaceutical Workflow For Development To QC</strong></h3>
<h5><strong>10:15 a.m. (IST) Lifecycle Management and QbD–An Analytical Perspective</strong></h5>
<ul>
<li>Kuldeep Sharma (Business Development Manager –Pharmaceutical)</li>
<li>Sreelakshmy Menon (Application Specialist –LCAgilent Technologies)</li>
</ul>
<h5><strong>11:15 a.m. (IST) One Instrument Multiple Possibilities: Cary 3500 Uv-vis With OpenlabECM Network Connectivity</strong></h5>
<ul>
<li>Shubham Sengupta (Product Specialist –Spectroscopy, Agilent Technologies)</li>
</ul>
<h5><strong>12:00 p.m. (IST) High Throughput Raman Spectroscopy from Raw Material Testing to Finished Product Analysis</strong></h5>
<ul>
<li>Shubham Sengupta (Product Specialist –Spectroscopy, Agilent Technologies)</li>
</ul>
<h5><strong>02:00 p.m. (IST) An Integrated Laboratory Informatics System for Greater Efficiency and Data Integrity</strong></h5>
<ul>
<li>Amit Ghate (Application Specialist –Lab Informatics, Agilent Technologies)</li>
</ul>
<h5><strong>03:00 p.m. (IST) A Guide to Updating HPLC Compendial Methods in Pharmaceutical Analysis</strong></h5>
<ul>
<li>Sunil Lakhmapure (Technical Support Specialist -Chemistries &amp; Supplies Division, Agilent Technologies)</li>
</ul>
<h5><strong>04:00 p.m. (IST) Compliance And CSV Solutions For Organizations To Comply With The Current Regulatory Requirements</strong></h5>
<ul>
<li>Sridhar Atmakuri (Sales Development Manager –Compliance Specialist, Agilent Technologies)</li>
</ul>


Agilent Technologies: Agilent Pharma Virtual Symposium 2022

Agilent Pharma Virtual Symposium 2022 - Day 1 - Pharmaceutical Workflow For Development To QC

Come and explore the world of pharmaceutical solutions which have been developed keeping your daily problems in mind.

Pharmaceutical Workflow For Development To QC

<p><strong>A cathode’s active material is composed of lithium and, in the majority of the cases, one or several metals. Proportion and content of the main elements in cathode material can affect the performance and cost of the lithium battery significantly, and the content of impurities in the material alters the safety of the battery. Conclusively, accurate determination and quantification of the main elements, as well as trace impurities, becomes particularly important.</strong></p>
<p>Evaluation of batteries and battery components requires a variety of analytical methods that study materials and component surfaces at various scales. Common elemental analysis techniques are inductively coupled plasma optical emission spectrometry (<strong>ICP-OES</strong>) and mass spectrometry (<strong>ICP-MS</strong>) or structural analysis with electron microscopy (<strong>SEM</strong>). But also other techniques as <strong>FTIR</strong>, <strong>Raman</strong> and <strong>NIR</strong> are used.</p>
<p>In this webinar session we will highlight the benefits of several analytical techniques, including ICP-OES and SEM for battery cathode material and structural analysis. </p>
<h5><strong>Learning points:</strong></h5>
<ul>
<li>Learn about analytical solutions for lithium-ion battery material and structural analysis</li>
<li>Learn how IC, GC-MS, ICP-OES, and SEM support battery value chain from raw materials to recycling</li>
<li>Learn about different applications and performance demonstrated with selected analysis examples</li>
</ul>
<h5><strong>Who should attend:</strong></h5>
<ul>
<li>Battery material analysis laboratory managers and analysts</li>
<li>Battery cell manufacturers and their QA/QC personnel</li>
<li>Scientists working in battery research and development</li>
</ul>
<blockquote>
<p><strong>Presenter: Simon Nelms (Product Marketing Manager, Thermo Fisher Scientific)</strong></p>
</blockquote>
<blockquote>
<p>Simon joined Thermo Fisher Scientific in 1996 as an applications specialist for ICP-MS, before taking a 2-year postdoctoral sabbatical at IRMM in Belgium. He re-joined the company in 2000 and in 2014 moved into Regional Marketing for the EMEA area. Simon has recently joined the Product Marketing team, covering trace elemental analysis accessories and software.</p>
</blockquote>
<blockquote>
<p><strong>Presenter: Tomoko Vincent (Application Specialist, Thermo Fisher Scientific)</strong></p>
</blockquote>
<blockquote>
<p>Tomoko gained 10 years’ experience of ICP-MS (single quad and sector field ICP-MS) for the industrial research laboratory in Japan. In 2007, moved to the position of Application Specialist for ICP-MS at Thermo Fisher Scientific in Bremen where she supports the customer with the development and implementation of new methods and regulations in their laboratory.</p>
</blockquote>
<blockquote>
<p><strong>Presenter: Letian Li (Market Development Manager, Thermo Fisher Scientific)</strong></p>
</blockquote>
<blockquote>
<p>Experienced Electron Microscopist focusing on scanning electron microscopy (SEM) and DualBeam instruments, with a solid background in applications of FIB/PFIB, Nanomaterials, Dual beam systems, Metallography in Materials Sciences. Skilled professional focused in Materials Engineering and PhD from Loughborough University. Looking forward to developing and enhancing electron microscopy applications for battery research and industry.</p>
</blockquote>


Thermo Scientific: PowerUp: Solutions for lithium-ion battery material analysis and testing

Analysis of battery cathode materials

We will highlight the benefits of several analytical techniques, including ICP-OES and SEM for battery cathode material and structural analysis.

<p><strong>Monitoring the quality of hydraulic and/or lube oils is critical to prevent premature wear of any kind of machinery. In this session we will look at this topic from a new perspective focusing on the combination of titration (potentiometric, thermometric, coulometric Karl Fischer titration) and Vis-Near-Infrared Spectroscopy (Vis-NIRS).</strong></p>
<p>Combining titration (highly sensitive, specific, a widely used primary method) with Vis-NIRS (fast, non-destructive, results for multiple parameters at once) can make your oil condition monitoring and/or lubricant analysis much more efficient, especially, if your laboratory has to analyze large sample series every day.</p>
<p>Attending this session, you will learn and understand:</p>
<ul>
<li>The specific advantages of each method (titration and Vis-NIR-Spectroscopy)</li>
<li>How and when to use these methods to measure critical chemical and physical parameters in lube and hydraulic oils</li>
<li>What thermometric titration is and how it helps to improve robustness of serial acid number testing</li>
<li>How to automate measurements of large sample series to increase efficiency and reproducibility</li>
<li>How Vis-NIRS for lubricant analysis complies with ASTM guidelines and can save costs and time</li>
</ul>
<blockquote>
<p><strong>Presenter:</strong> Robert Tobler (Application Specialist Titration)</p>
</blockquote>
<blockquote>
<p>Robert Tobler studied chemistry at the Zurich University of Applied Science in Wädenswil, Switzerland. He joined Metrohm in 2015 as an application specialist titration. Since 2018 he has also been involved in stability measurement.</p>
</blockquote>
<blockquote>
<p><strong>Presenter:</strong> Nicolas Rühl, PhD (Product Manager Spectroscopy)</p>
</blockquote>
<blockquote>
<p>Dr. Nicolas Rühl is working in the Competence Center Spectroscopy since 2015. In this time, he has been in charge of developing the near-infrared (NIR) spectroscopy business at Metrohm. Nicolas has a Master in Business Administration and received his PhD in physical chemistry on single-molecule spectroscopy using Vis-NIR and Raman spectroscopy technologies.</p>
</blockquote>
<blockquote>
<p><strong>Moderator:</strong> Tom Lynch CChem FRSC (Independent Analytical Consultant, International Labmate)</p>
</blockquote>
<blockquote>
<p>Tom has 35 years of experience in the petroleum industry, specialising in the delivery of forensic and problem solving /method development capabilities for BP Fuels and Lubricants businesses globally. He was also a member of the BP Science Council representing Analytical Science and led a BP wide Analytical Science network.Tom has published over 30 citable papers, 4 book chapters and has given over 60 presentations at conferences. He is a past Vice President of the Royal Society of Chemistry (RSC) Analytical Division and a past Chairman of the RSC Separation Science Group. In addition, Tom is a recipient of the Silver Jubilee Medal by the Chromatographic Society and a technical achievement award by the Energy Institute.</p>
</blockquote>


Metrohm: Making your quality control of hydraulic and lube oils more efficient

Making your quality control of hydraulic and lube oils more efficient

Combining titration and Vis-Near-Infrared Spectroscopy for higher sample throughput & faster results

Efficient quality control of hydraulic and lube oils

<p><strong>Characterization of geological materials, including elemental composition, chemical speciation, and phase determination, is of primary importance for assessing their natural resources as well as their exploration, beneficiation, and extraction processes for industrial needs.</strong></p>
<p>X-ray techniques, including X-ray fluorescence (XRF) and X-ray diffraction (XRD), have long been essential tools in geological research. Due to the relatively quick and simple sample preparation, XRF has become the technique of choice for the analysis of rocks and minerals. New generations of XRF analyzers also permit analysis of small spots down to 0.5 mm as well as mapping of a selected area of a sample. These new possibilities open up the XRF technique to heterogeneous samples where segregations, defects, or inclusions can now be determined. Coupling these capabilities with standard-less analysis allows quantification of up to 79 elements of the periodic table on selected points or areas of the sample. On the other hand, XRD measurements of crystalline materials in combination with Rietveld refinement is widely recognized as the most powerful method for quantitative crystalline-phase analysis.</p>
<p>Deriving chemical and structural information from the fundamental vibrations of molecular bonds, Fourier transform infrared spectroscopy (FTIR) and Raman spectroscopy also find many applications in geosciences research, including identification of minerals and their polymorphic forms, differentiation from other organic and inorganic materials, qualitative and quantitative determination of structural incorporated molecules and defects, characterization of thermal maturity, etc.</p>
<p>In this presentation, several real-world geological applications using X-ray and vibrational spectroscopic techniques will be presented. The complementarity of different analytical techniques will also be discussed.</p>
<blockquote>
<p><strong>Presenter:</strong> Christopher Shaffer (Business Development Manager, Thermo Fisher Scientific)</p>
</blockquote>
<blockquote>
<p>Chris is the Business Development Manager for the Thermo Fisher Scientific Bulk Element Analysis (BEA) Division (x-ray diffraction, x-ray fluorescence and optical emission spectroscopy). He has been with the BEA business since 2007. After graduating from college, Chris started his career at the Ferro Corporation managing an analytical laboratory, where he first learned the techniques of x-ray diffraction (XRD) and x-ray fluorescence (XRF). Chris left Ferro to join Thermo Fisher Scientific as an XRF applications specialist for North America. In 2011, he moved to Switzerland to become the product manager for the newly launched Thermo Scientific™ ARL™ Perform’X XRF. In 2013, Chris moved back to North America as Latin American business manager for the BEA group and in 2017, he moved to his current position.</p>
</blockquote>
<blockquote>
<p><strong>Presenter:</strong> Rui Chen (Applications Manager, Spectroscopy, Thermo Fisher Scientific)</p>
</blockquote>
<blockquote>
<p>Dr. Rui Chen obtained his Ph.D. in analytical chemistry from the University of Alberta, Canada, followed by an Alberta Ingenuity Postdoctoral fellowship. Rui has extensive experience in a wide range of analytical techniques including chromatography, mass spectrometry, and vibrational spectroscopy. Currently, he is the senior manager of the applications team at Thermo Fisher Scientific supporting vibrational spectroscopy, optical emission spectroscopy, x-ray fluorescence, x-ray diffraction, extrusion, and rheology product lines.</p>
</blockquote>


Thermo Scientific: Geological Applications Using XRF, XRD and Vibrational Spectroscopy

Geological Applications Using XRF, XRD and Vibrational Spectroscopy

Several real-world geological applications using X-ray and vibrational spectroscopic techniques.

Geological Applications Using XRF, XRD

<p><strong>In this 4-part session you will gain insights and understanding of what you can do in the battery industry with varied technologies. From investigating solutes and electrodes, following battery cell behavior, and in situ research on energy storage materials the Bruker Scientists are sharing a wealth of knowledge for your research.</strong></p><p><strong>Session 1: 11:00 a.m.</strong></p><h5><strong>Powering the Future: Analytical Methods in Battery Research</strong></h5><p>Chemical understanding of batteries is essential for enhancing their performance, longevity, and safety. This session will highlight the role that analytical techniques play in battery research and development. By offering deep insights into the chemical, structural, and electrochemical properties of energy storage materials, these methods enable researchers to drive innovation and solve complex challenges. We'll provide an overview of key analytical approaches, including spectroscopy, solid-state NMR, and X-ray diffraction, and discuss their applications in advancing battery technology.</p><p><strong>Session 2: 11:25 a.m.</strong></p><h5><strong>Spectroelectrochemical Setup for Probing Reactions on Electrodes and in Electrolytes</strong></h5><p>Electrochemistry combined with vibrational spectroscopy provides powerful insights into electrochemical reactions and battery research through unique infrared and Raman signatures. The session will cover accessories, setup optimization, and applications like electro-oxidation of metal-organic complexes and lithium battery interface mapping.</p><p><strong>Session 3: 11:50 a.m.</strong></p><h5><strong>Advancements and Challenges of Solid-State NMR Technology for Battery Research</strong></h5><p>Solid-State Nuclear magnetic resonance (NMR) is a characterization technique applied to investigate the structural changes of/in battery materials. Advanced NMR approaches can be used to track and examine ion-exchange/diffusion across interfaces, electrolyte decomposition, dendrite formation, storage behavior of an electrode etc. during or following charging/discharging in order to understand electrochemical processes and improve battery properties.</p><p><strong>Session 4: 12:15 p.m.</strong></p><h5><strong>Charge and Structure: Understanding Batteries Through X-Ray Diffraction</strong></h5><p>X-ray diffraction (XRD) serves as a powerful tool for elucidating the structural properties of battery materials at the atomic scale. Modern XRD techniques can be used to understand the effects of cycling and synthesis methods on electrode stability and efficiency, ultimately guiding the development of next-generation energy storage solutions.</p><p><strong>Key Learning Objectives:</strong></p><ul><li>Gain an overview of current trends in battery technology.</li><li>Understand the key components of battery chemistry and design.</li><li>Learn about future trends in battery development and energy storage.</li></ul><p><strong>Who Should Attend:</strong></p><ul><li>Laboratory managers</li><li>Batteries developers</li><li>Electrochemical researchers</li></ul><blockquote><p><strong>Presenter:</strong> Federico Paruzzo, PhD (Academic Market Project Manager, Bruker BBIO)</p><p><strong>Presenter: </strong>Sergey Shilov, PhD (NA Product Manager, Science, Bruker Optics)</p><p><strong>Presenter: </strong>Edina Sic (Solutions Product Manager, Academic Battery Research, Bruker BioSpin Group)</p><p><strong>Presenter: </strong>Nick Rodesney (XRD Applications Scientist, Bruker)</p><p><strong>Presenter:</strong> Ann Thayer (Contributing Editor, C&amp;EN Media Group)</p></blockquote>

The Science of Batteries

In this 4-part session you will gain insights and understanding of what you can do in the battery industry with varied technologies.

<div><div dir="" aria-atomic="true"><p id="isPasted"><strong>As petrochemical companies strive to enhance operational efficiency, finding an intersection between industry standards and process innovation is essential for sustainable growth. At the same time, there is pressure to lower costs in order to achieve a competitive advantage in an evolving market.</strong></p><p>In this webinar, Larry Tucker, Secretary Chairperson of Subcommittee 6 on Liquid Fuels and Lubricants, as well as Vice Chair of Subcommittee 3 on Inorganic Analysis for ASTM, will provide insights into the latest updates of ASTM D6122 and D8340. Elena Hagemann, Product Manager for Process Spectroscopy at Metrohm USA, will discuss recent advancements in process spectroscopy and their integration with Process Analytical Technology (PAT). Leave with an understanding on how to make smarter decisions to achieve a competitive advantage in the petrochemical landscape.</p><p id="isPasted"><strong fr-original-style="">Who should attend?</strong></p><ul><li>Production managers</li><li>Product development scientists</li><li>Process engineers</li><li>Operational managers</li><li>Quality control specialists&nbsp;</li><li>Plant manager</li></ul><p><strong fr-original-style="">Key learning points&nbsp;</strong></p><ul><li>Learn how Spectroscopy PAT can be applied to optimize processes, ensuring better quality and efficiency.</li><li>Gain a thorough understanding of ASTM D6122 and D8340, including recent updates and their impact on petrochemical applications.</li><li>Explore strategies to stay ahead of competitors by combining spectroscopy with ASTM standards for optimized performance and compliance.</li></ul><div><div dir=""><div><blockquote><div><strong>Presenter:</strong> Larry Tucker (Director of Norms and Standards, Metrohm USA)</div></blockquote></div></div></div><div><blockquote><p align="LEFT">Larry Tucker is the Director of Norms and Standards at Metrohm USA. In his 40-year career, Larry has held positions in sales, marketing and business development, as well as management. In his current role, Larry works with industry partners to improve and develop new test methods in the petroleum, environmental, pharmaceutical and food markets. He actively participates in ASTM Committee D02 Petroleum Products, Liquid Fuels and Lubricants where he serves as Secretary. He's also chairperson of subcommittee 6 Liquid Fuels and Lubricants. He has led and participated in the development and improvement of numerous ASTM test methods and standards. Larry received his B.S in Chemistry from the University of West FL and has over 35 years of industry experience in developing analytical test methods.</p></blockquote><div><div dir=""><div><blockquote><div><strong>Presenter: </strong>Elena Hagemann (Process Spectroscopy Product Manager, Metrohm USA)</div></blockquote></div></div></div><div><blockquote><p>Elena Hagemann is the Product Manager for Process Spectroscopy at Metrohm USA in Riverview, Florida. She earned her Master degree in Analytical and Bioanalytical Chemistry at the Applied University of Aalen, Germany, where she completed her studies with her Master thesis focused on Karl Fischer Titration, NIR Spectroscopy and Multivariate Data Analysis. Elena joined the Metrohm Group in August 2013 and started with Metrohm USA in January of 2018, focusing on Raman and NIR Spectroscopy. She performs internal as well as customer training.</p></blockquote></div></div></div></div>

Metrohm: Leveraging ASTM D6122 & D8340 for a Competitive Edge in Petrochemicals

Leveraging ASTM D6122 & D8340 for a Competitive Edge in Petrochemicals

We will discuss recent advancements in process spectroscopy and their integration with Process Analytical Technology (PAT).

ASTM D6122 & D8340 for a Competitive Edge in Petrochemicals

<p><strong>Accurate protein concentration measurement is critical in biochemical and biophysical research. A powerful UV-Vis spectrophotometer can streamline this process, enabling rapid and precise determination of protein extinction coefficients. Intuitive software allows users to simplify extinction coefficient calculations using the Beer-Lambert law equation—eliminating complexity with just one click.</strong></p><p>Join us for an insightful webinar on how the Cary 3500 UV-Vis Multicell Pelter streamlines this process, enabling rapid and precise determination of protein extinction coefficients at 280 nm.</p><p>Learn how this innovative system supports Biopharma applications, including the analysis of innovator and biosimilar proteins.Additionally, explore how built-in calibration curves facilitate monoclonal antibody (mAb) concentration estimation during bioprocessing.</p><p>This session will provide practical insights, making it a must-attend event for researchers, analysts, and quality control professionals seeking to enhance their workflows with cutting-edge UV-Vis technology.</p><h4><strong>What you will learn:</strong></h4><ul><li>Understand the fundamentals of protein extinction coefficients and concentration analysis</li><li>Explore the Cary Workstation software features that enable one-click calculation of protein extinction coefficients</li><li>Learn how the Cary 3500 UV-Vis Multicell Pelter optimizes efficiency by simultaneously measuring multiple samples</li><li>Discover built-in software capabilities, including calibration curve development and concentration estimation for bioprocessing applications</li></ul><h4><strong>Who Should Attend:</strong></h4><ul><li>Analytical scientists and technicians using UV-Vis technologies</li><li>Researchers working with proteins, peptides, or biopharmaceuticals</li><li>Quality control specialists in biopharma and related industries</li><li>Laboratory managers looking to enhance analytical efficiency and accuracy</li></ul><blockquote><p><strong>Presenter</strong>: Aveline Neo, PhD (Solution Scientist, Agilent Technologies, Inc.)</p><p>Aveline Neo boasts an impressive background in biology and analytical science. She earned her PhD from the National University of Singapore and began her career at Agilent in 2012, where she focused on lipidomics using liquid chromatography and mass spectrometry.</p><p>After completing post-doctoral research at the Babraham Institute in Cambridge, she returned to Agilent as a solution scientist in the Global Solution Development Center. Over the years, she has contributed to various projects involving recombinant proteins, alternative proteins, mRNA, and monoclonal antibodies.</p><p>Aveline has demonstrated expertise in analytical techniques, including liquid chromatography, mass spectrometry, and spectroscopic methods such as UV-Vis, FTIR, and Raman.</p><p><strong>Moderator</strong>: Michelle Taylor (Editor-in-Chief, Labcompare | Laboratory Equipment)</p></blockquote>

Agilent Technoloies: Simplify Your Workflow: Rapid and Efficient Protein Analysis with UV-Vis Spectroscopy

Simplify Your Workflow: Rapid and Efficient Protein Analysis with UV-Vis Spectroscopy

How the Cary 3500 UV-Vis Multicell Pelter streamlines this process, enabling rapid and precise determination of protein extinction coefficients at 280 nm

Protein Analysis with UV-Vis Spectroscopy

<p><strong>Traditional wet chemistry methods for food testing tend to be slow and wasteful. In contrast, near-infrared spectroscopy (NIRS) is chemical-free and can be used to determine multiple QC parameters in a few seconds with a single measurement.</strong></p><p>Join us for a free webinar on September 25, where Dr. Nicolas Rühl, Product Manager Spectroscopy, and Andreas Agerer, Application Specialist Spectroscopy at Metrohm International Headquarters, will introduce NIRS and explore its wide range of applications for food quality control.</p><p>In short laboratory demonstrations, the presenters will showcase the analysis of moisture, fat, protein, and other food parameters using the newly released OMNIS NIR Analyzer. Highlighting key features such as intuitive measurement workflows, calibration at the push of a button, and fully automated analysis of more than 200 samples, the presenters will show you how to boost your food testing to a whole new level of performance.</p><p><strong>Don't miss this opportunity and register today!</strong></p><h5><strong>Join us for this event and learn:</strong></h5><ul><li>What NIR spectroscopy is and how it works</li><li>How to perform NIR analysis to determine typical food quality parameters</li><li>How NIR spectroscopy helps you save time and costs of your routine food testing</li><li>How unique features of the OMNIS NIR Analyzer make NIR analysis easy to use for everyone</li></ul><h5><strong>Who should attend?</strong></h5><ul><li>QC and QA managers from the food industry, lab managers, lab technicians</li></ul><blockquote><p><strong>Presenter: </strong>Dr. Nicolas Rühl (Product Manager Spectroscopy, Metrohm International Headquarters)</p><p>Dr. Nicolas Rühl works at the Competence Center Spectroscopy at Metrohm International Headquarters since 2015. In this time, he has been in charge of developing the near-infrared (NIR) spectroscopy business at Metrohm. Nicolas has a Master in Business Administration and received his PhD in physical chemistry on single-molecule spectroscopy using Vis-NIR and Raman spectroscopy technologies.</p><p><strong>Presenter: </strong>Andreas Agerer (Application Specialist NIRS, Metrohm International Headquarters)</p><p>Andreas Agerer is an Application Specialist at Metrohm AG, working in the Competence Center Spectroscopy since 2018. In this time, he has been responsible for developing NIRS methods tailored to new application areas and supporting sales teams during feasibility studies. Andreas completed his university graduate work in the field of polymer analysis using vibrational spectroscopy.</p></blockquote>

Metrohm: Next-generation NIR spectroscopy and how to use it for high-throughput food testing

Next-generation NIR spectroscopy and how to use it for high-throughput food testing

Join Metrohm’s webinar to explore NIR spectroscopy for food QC. See how the OMNIS NIR Analyzer delivers fast, chemical-free analysis of key food parameters.

Next-generation NIR spectroscopy for food testing

<div><div id="inner_content_body_text" data-content-id="394785"><p><strong>In response to growing environmental concerns and the urgent need for sustainable practices, the upcycling of post-consumer and reprocessed plastics has become a critical focus. This webinar will delve into the upcycling of reprocessed polypropylene (rPP) through reactive extrusion, emphasizing the use of a compatibilizer and the optimization of key process variables.</strong></p><h4><strong>Key Topics Covered:</strong></h4><ul><li>Optimization of Extrusion Parameters: Learn how factorial design of experiment techniques can be utilized to assess and optimize important extrusion parameters.</li><li>Rheological Testing: Discover how rheological measurements can evaluate polymer structure, processability, and performance.</li><li>FTIR Microscopy Mapping: Explore how FTIR microscopy mapping aids in understanding the structure of polymer blends.</li><li>Compatibilizer Benefits: Gain insights into how the addition of a compatibilizer can improve the mechanical properties of immiscible polymer blends.&nbsp;</li></ul><h4><strong>Attend This Webinar to:</strong></h4><ul><li>Enhance your knowledge of polymer upcycling and reactive extrusion.</li><li>Learn about cutting-edge analytical techniques for evaluating key process parameters.</li><li>Discover how to optimize polymer processing for improved sustainability and performance.</li></ul><h4><strong>Ideal For Those Who:</strong></h4><ul><li>Explore advanced methods for polymer recycling.</li><li>Develop eco-friendly processing technologies.</li><li>Optimize workflows for circular material use.</li><li>Apply cutting-edge techniques for polymer analysis.</li><li>Implement scalable, sustainable recycling solutions.</li><li>Want to gain insight into next-generation polymer recovery.</li></ul><blockquote><p><strong>Presenter:</strong> Lucivan Barros, Ph.D., Senior Applications Scientist, Thermo Fisher Scientific</p><p>Lucivan Barros is a Senior Applications Scientist at Thermo Fisher Scientific, specializing in extrusion and rheology applications. He earned his Ph.D. in Macromolecular Science from Case Western Reserve University. With expertise in polymer processing, materials development, and structure–property relationships, he is dedicated to advancing sustainable materials and supporting innovation in polymer processing and characterization.</p><p><strong>Presenter: </strong>Ron Rubinovitz, Ph.D., Senior Applications Scientist, Thermo Fisher Scientific</p><p>Ron Rubinovitz, Ph.D. is a Senior Applications Scientist with 14 years of experience at Thermo Fisher Scientific working with FT-IR applications including FT-IR microscopy, FT-Raman spectroscopy and chemometrics. &nbsp;Ron obtained his Ph.D. in physical chemistry at the University of Pennsylvania utilizing FTIR and continues to use the benefits of the FTIR techniques in numerous applications.</p></blockquote></div></div>

Thermo Fisher Scientific: Polymer Upcycling via Reactive Extrusion: FTIR Microscopy Insights into Blend Compatibilization

Polymer Upcycling via Reactive Extrusion: FTIR Microscopy Insights into Blend Compatibilization

Join Thermo to explore reactive extrusion, FTIR mapping, and compatibilizer effects for efficient, sustainable polymer upcycling and improved blend quality.

Polymer Upcycling: FTIR Microscopy Insights

<div><p><strong>Discover how KnowItAll streamlines structure elucidation workflows, spectrum-to-spectrum comparison, and identification of unknown peaks. With intelligent, user-friendly NMR tools designed for real-world spectroscopy challenges.&nbsp;</strong></p><h5><strong>In this webinar, you'll:&nbsp;</strong></h5><ul><li>Explore intuitive processing, analysis, and prediction tools for H-, C-, and X-NMR&nbsp;</li><li>Discover what's new in KnowItAll 2026's NMR-specific updates&nbsp;</li><li>Learn a novel searching approach for multi-technique laboratories&nbsp;</li></ul><p>Learn how KnowItAll's NMR package solves your spectroscopy challenges with a comprehensive toolkit designed to support a wide range of users, from undergraduate courses to professional laboratories.&nbsp;</p><h4><strong>About Wiley’s KnowItAll Software&nbsp;</strong></h4><p>KnowItAll offers complete solutions to identify, analyze, and manage your NMR data. Combined with Wiley’s comprehensive, high-quality spectral reference databases, it provides one of the most advanced technologies available for fast, reliable spectral analysis. &nbsp;</p><p>KnowItAll supports multiple techniques and instrument vendor formats. So, whether you use just NMR or additional spectral techniques (GC-MS, LC-MS, IR, Raman, UV-Vis), it’s the ideal vendor neutral solution for your lab.&nbsp;</p><blockquote><p><strong>Presenter:</strong> Michelle D’Souza, PhD (Product Manager, Software Products, Wiley Science Solutions, Wiley)</p><p>Dr. D’Souza brings years of insight and knowledge in the area of spectral informatics with leadership roles at both Wiley and Bio-Rad Laboratories. In addition to her multiple years as a scientific researcher at Abbott (now AbbVie) and DuPont, she has a Ph.D. in Chemistry from Northern Illinois University and a Masters in Analytical Chemistry from the Chinese Academy of Preventative Medicine. She earned a BS degree from Chemistry Department of Beijing University. &nbsp;</p><p><strong>Presenter:</strong> Nadia Martina, Ph.D. (Product Manager, Software &amp; Databases – New Techniques, Wiley Science Solutions, Wiley)</p><p>Dr. Nadia Martina is a Product Manager for Wiley Science Solutions, where she oversees the development of new products and databases, while supporting existing KnowItAll capabilities. She earned her Ph.D. in Materials Science from Ontario Tech University, where she executed chemistry research using a variety of instrumental analytical techniques. Since joining Wiley in 2022, Nadia has focused on cheminformatics and software development.</p></blockquote></div>

Wiley: NMR simplified: Process, identify, predict, & database with confidence

NMR simplified: Process, identify, predict, & database with confidence

Discover how KnowItAll streamlines structure elucidation workflows, spectrum-to-spectrum comparison, and identification of unknown peaks.